Published January 2016 | Version v1
Journal article

A simple approach to atom probe sample preparation by using shadow masks

  • 1. Australian Centre for Microscopy and Microanalysis, The University of Sydney, 2006 (Australia)
  • 2. Materials Department, University of California, Santa Barbara, 93106-5050 (United States)

Description

Here, we present a new method that utilises shadow masks in a broad ion beam system to prepare atom probe samples. It is particularly suited to non-conductors and materials with surface layers such as surface oxides, implanted layers or thin films. This new approach bypasses the focused ion beam (FIB) lift-out step, increasing the sample throughput, dramatically reducing the required FIB beam time and decreasing the complexity of sample preparation. - Highlights: • Atom probe samples can be fabricated using a broad ion beam with a shadow mask. • Only a short amount of FIB is required to sharpen the sample. • Samples can be re-used by applying a second shadow mask.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.ultramic.2015.09.005

Additional details

Identifiers

DOI
10.1016/j.ultramic.2015.09.005;
PII
S0304-3991(15)30028-0;

Publishing Information

Journal Title
Ultramicroscopy (Amsterdam)
Journal Volume
160
Journal Page Range
p. 163-167
ISSN
0304-3991
CODEN
ULTRD6

INIS

Country of Publication
Netherlands
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
48021789
Subject category
S36: MATERIALS SCIENCE;
Descriptors DEI
ATOMS; ION BEAMS; IONS; LAYERS; OXIDES; PROBES; SAMPLE PREPARATION; SURFACES; THIN FILMS; TOMOGRAPHY
Descriptors DEC
BEAMS; CHALCOGENIDES; CHARGED PARTICLES; DIAGNOSTIC TECHNIQUES; FILMS; OXYGEN COMPOUNDS

Optional Information

Copyright
Copyright (c) 2015 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.