Published January 2016
| Version v1
Journal article
A simple approach to atom probe sample preparation by using shadow masks
- 1. Australian Centre for Microscopy and Microanalysis, The University of Sydney, 2006 (Australia)
- 2. Materials Department, University of California, Santa Barbara, 93106-5050 (United States)
Description
Here, we present a new method that utilises shadow masks in a broad ion beam system to prepare atom probe samples. It is particularly suited to non-conductors and materials with surface layers such as surface oxides, implanted layers or thin films. This new approach bypasses the focused ion beam (FIB) lift-out step, increasing the sample throughput, dramatically reducing the required FIB beam time and decreasing the complexity of sample preparation. - Highlights: • Atom probe samples can be fabricated using a broad ion beam with a shadow mask. • Only a short amount of FIB is required to sharpen the sample. • Samples can be re-used by applying a second shadow mask.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.ultramic.2015.09.005Additional details
Identifiers
- DOI
- 10.1016/j.ultramic.2015.09.005;
- PII
- S0304-3991(15)30028-0;
Publishing Information
- Journal Title
- Ultramicroscopy (Amsterdam)
- Journal Volume
- 160
- Journal Page Range
- p. 163-167
- ISSN
- 0304-3991
- CODEN
- ULTRD6
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 48021789
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- ATOMS; ION BEAMS; IONS; LAYERS; OXIDES; PROBES; SAMPLE PREPARATION; SURFACES; THIN FILMS; TOMOGRAPHY
- Descriptors DEC
- BEAMS; CHALCOGENIDES; CHARGED PARTICLES; DIAGNOSTIC TECHNIQUES; FILMS; OXYGEN COMPOUNDS
Optional Information
- Copyright
- Copyright (c) 2015 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.