Published 1994 | Version v1
Miscellaneous

Zirconium tetrachloride production using the fluidized bed chlorination technique

  • 1. Instituto de Pesquisas Energeticas e Nucleares (IPEN), Sao Paulo, SP (Brazil)

Description

In this paper the results of a study of the process for production nuclear grade zirconium tetrachloride by fluidized bed chlorination technique are presented. A reactor with a gas distributor has been developed and this permitted to establish a procedure of zirconium tetrachloride production with adequate purity, satisfactories efficiency of reaction and reproducible results. Some relevant parameters of the kinetics of chlorination process such as: time and temperature of reaction, size and minimum fluidizing velocity of microspheres and percentage of the reducing agent have been studied. (author). 15 refs., 5 figs

Availability note (English)

Available from the Nuclear Information Center of Brazilian Nuclear Energy Commission, Rio de Janeiro.

Additional details

Additional titles

Original title (Portuguese)
Obtencao de tetracloreto de zirconio pela tecnica de cloracao em leito fluidizado

Publishing Information

Imprint Pagination
3 p.

Conference

Title
11. Brazilian Congress on Engineering and Materials Science.
Original Conference Title
11. Congresso Brasileiro de Engenharia e Ciencia dos Materiais
Dates
11-14 Dec 1994.
Place
Aguas de Sao Pedro, SP (Brazil).

INIS

Country of Publication
Brazil
Country of Input or Organization
Brazil
INIS RN
28027349
Subject category
S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; S36: MATERIALS SCIENCE;
Resource subtype / Literary indicator
Conference, Non-conventional Literature
Descriptors DEI
CHEMICAL REACTIONS; CHLORINATION; FLUIDIZED BEDS; MATERIALS; ZIRCONIUM; ZIRCONIUM CHLORIDES
Descriptors DEC
CHLORIDES; CHLORINE COMPOUNDS; ELEMENTS; HALIDES; HALOGEN COMPOUNDS; HALOGENATION; METALS; TRANSITION ELEMENT COMPOUNDS; TRANSITION ELEMENTS; ZIRCONIUM COMPOUNDS