Published December 2024 | Version v1
Journal article

Performance assessment of elemental characterization in environmental samples at the KRISS-KAERI INAA laboratory

  • 1. KRISS-KAERI Joint Research Center for Reference Materials Using Research Reactor, KRISS and KAERI, Daejeon (Korea, Republic of)
  • 2. Gyeongsang National University, Jinju (Korea, Republic of). The Research Institute of Natural Science
  • 3. Korea Research Institute of Standards and Science (KRISS), Daejeon (Korea, Republic of). Division of Chemical and Material Metrology
  • 4. Korea Atomic Energy Research Institute (KAERI), Daejeon (Korea, Republic of). Hanaro Utilization Division

Description

Verification of analytical laboratory performance is essential to ensure the analytical procedure adopted to obtain reliable results. The KRISS-KAERI joint research center participated in IAEA proficiency tests to verify the analytical performance of the laboratory, specifically for the INAA technique. A forty major, minor, and trace elements in siliceous and plant matrix samples were analyzed using standard calibrator INAA, relative INAA, k0-INAA, and WD-XRF methods. Statistical metrics such as z- or z'-score, zeta score, and R-score were calculated based on assigned values for elements. We achieved a good score, with less than 2 in statistical matrices for most elements, which confirmed the capabilities of methodology procedure used in the KRISS-KAERI INAA laboratory. (author)

Additional details

Publishing Information

Journal Title
Journal of Radioanalytical and Nuclear Chemistry
Journal Volume
333
Journal Issue
12
Journal Page Range
p. 6669-6678
ISSN
0236-5731
CODEN
JRNCDM

Conference

Title
16. International Conference on Modern Trends in Activation Analysis
Acronym
MTAA-16
Dates
5-10 May 2024
Place
Budapest (Hungary)

INIS

Country of Publication
Hungary
Country of Input or Organization
Hungary
INIS RN
56006968
Subject category
S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
Resource subtype / Literary indicator
Conference
Descriptors DEI
LABORATORIES; MEASURING INSTRUMENTS; NEUTRON ACTIVATION ANALYSIS; NEUTRON ACTIVATION ANALYZERS; QUALITY CONTROL; X-RAY FLUORESCENCE ANALYSIS
Descriptors DEC
ACTIVATION ANALYSIS; CHEMICAL ANALYSIS; CONTROL; MEASURING INSTRUMENTS; NONDESTRUCTIVE ANALYSIS; X-RAY EMISSION ANALYSIS

Optional Information

Notes
20 refs.