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Published October 2019 | Version v1
Journal article

Complexes of Cobalt and Copper Halides Based on 1,3-Dimethylimidazolium-4-Carboxylate

  • 1. Russian Academy of Sciences, Kurnakov Institute of General and Inorganic Chemistry (Russian Federation)
  • 2. Marshal V. I. Chuikov Moscow South-Eastern School (Russian Federation)

Description

In the interaction of norzooanemonin 1,3-dimethylimidazolium-4-carboxylate (1) with CuBr2, two types of crystals form: purple [Cu(L)2Br2][CuBr4][CuL4] (2) and light blue [CuL4][CuBr3] (3). In the reaction of 1 with CoCl2 in methanol, neutral complex Co(L)2Cl2 (4) forms. The thermal decomposition of complex 4 is studied. At the first stage of this decomposition, two equivalents of CO2 remove in a range 218–275 °C, and then a two-phase removal of two equivalents of L and the formation of CoCl2 occur.

Additional details

Identifiers

Publishing Information

Journal Title
Journal of Structural Chemistry
Journal Volume
60
Journal Issue
10
Journal Page Range
p. 1648-1654
ISSN
0022-4766
CODEN
JSTCAM

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Copyright
Copyright (c) 2019 Pleiades Publishing, Ltd.