Published April 1, 1988
| Version v1
Journal article
A heatable stretching device for dynamic X-ray studies
Creators
- 1. Technische Hogeschool Eindhoven (Netherlands). Dept. of Polymer Technology
- 2. DSM Research, Geleen (Netherlands)
Description
In this paper a heatable stretching device is presented which enables the performance of real-time X-ray experiments during deformation. The construction of the oven makes it possible to perform experiments with detectable X-ray diffraction angles (2θ) of up to 300. It is shown that the apparatus can be used to study morphological changes occurring during the deformation/drawing of polymer materials, using the benefits of synchrotron facilities. A series of small-angle (SAXS) and wide-angle (WAXS) X-ray scattering patterns obtained during the drawing of melt-crystallized ultra-high-molecular-weight polyethylene (UHMW-PE) at 373 K is presented. (orig.)
Additional details
Publishing Information
- Journal Title
- J. Appl. Crystallogr.
- Journal Volume
- 21
- Journal Issue
- 2
- Series
- J. Appl. Crystallogr.
- Journal Page Range
- 106-108
- ISSN
- 0021-8898
- CODEN
- JACGA
INIS
- Country of Publication
- Denmark
- Country of Input or Organization
- Denmark
- INIS RN
- 19090399
- Subject category
- S75: CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY;
- Descriptors DEI
- DEFORMATION; DRAWING; EQUIPMENT; HEATING; MATERIALS; MEDIUM TEMPERATURE; POLYETHYLENES; POLYMERS; SYNCHROTRON RADIATION; X-RAY DIFFRACTION; X-RAY DIFFRACTOMETERS
- Descriptors DEC
- BREMSSTRAHLUNG; COHERENT SCATTERING; DIFFRACTION; DIFFRACTOMETERS; ELECTROMAGNETIC RADIATION; FABRICATION; MATERIALS WORKING; MEASURING INSTRUMENTS; ORGANIC COMPOUNDS; ORGANIC POLYMERS; POLYOLEFINS; RADIATIONS; SCATTERING