Published January 1993 | Version v1
Journal article

Periodicity in the formation constant values of lanthanide (III) aminopolycarboxylate resorcinol/orcinol/phloroglucinol mixed ligand complexes

  • 1. Dr. H.S. Gour Vishwavidyalaya, Sagar (India). Dept. of Chemistry

Description

Formation constants (log Ksub(MAL)sup(MA) of mixed ligand complexes [Ln(III).A.L], where Ln(III) = La3+, Ce3+, Pr3+, Nd3+, Sm3+, Eu3+, Gd3+, Tb3+ or Dy3+; A = NTA, HEDTA or EDTA and L = resorcinol (res), orcinol (orc) or phloroglucinol (phl), have been determined pH-metrically using the Irving-Rossotti approach at 25oC and at an ionic strength, I=0.2(mole dm-3, NaClO4). The log Ksub(MAL)sup(MA) values lie in the sequence: (i) NTA>HEDTA>EDTA and (ii) orc>res>phl with respect to primary (A) and secondary (L) ligands, respectively. Periodicity has been observed in the formation constant values, which lie in the sequence La3+Gd<3+f3-f4 ≅ f10-f11. Hydration numbers (HN) of Ln(III) ions have been calculated; tetrad effect is present in HN. (author). 37 refs., 2 tabs., 2 figs

Additional details

Publishing Information

Journal Title
Proceedings - Indian Academy of Sciences. Chemical Sciences
Journal Volume
105
Journal Issue
3
Journal Page Range
p. 155-160.
ISSN
0253-4134
CODEN
PIAADM