Published March 5, 2014 | Version v1
Journal article

Recent developments in two fundamental aspects of electron backscatter diffraction

  • 1. National Physical Laboratory, Hampton Road, Teddington TW11 0LW (United Kingdom)
  • 2. Aunt Daisy Scientific, Claremont House, Lydney GL15 5DX (United Kingdom)

Description

Two very different aspects of electron backscatter diffraction (EBSD) are considered in this paper. Firstly, the use of the technique for the measurement of grain size is discussed with particular reference to the development of international standards to help ensure reproducible and repeatable measurements. In particular the lessons learnt for both calibration of the complete SEM-EBSD system and in choice of the correct data acquisition and processing parameters from an international round robin are summarized. Secondly, extending the capability of EBSD through development of new detectors is discussed. New shadow casting methods provide a means to achieve better accuracy in definition of sample-pattern geometry, while increased detail can be obtained by larger cameras and ultimately direct electron detection

Availability note (English)

Available from http://dx.doi.org/10.1088/1757-899X/55/1/012011

Additional details

Publishing Information

Journal Title
IOP Conference Series. Materials Science and Engineering (Online)
Journal Volume
55
Journal Issue
1
Journal Page Range
[12 p.]
ISSN
1757-899X

Conference

Title
13. European workshop on modern developments and applications in microbeam analysis
Acronym
EMAS 2013 workshop
Dates
12-16 May 2013
Place
Porto (Portugal)

INIS

Country of Publication
United Kingdom
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
47067474
Subject category
S36: MATERIALS SCIENCE;
Resource subtype / Literary indicator
Conference
Descriptors DEI
ACCURACY; BACKSCATTERING; CALIBRATION; CASTINGS; DATA ACQUISITION; ELECTRON DETECTION; ELECTRON DIFFRACTION; ELECTRONS; GRAIN SIZE; SCANNING ELECTRON MICROSCOPY
Descriptors DEC
CHARGED PARTICLE DETECTION; COHERENT SCATTERING; DATA PROCESSING; DETECTION; DIFFRACTION; ELECTRON MICROSCOPY; ELEMENTARY PARTICLES; FERMIONS; LEPTONS; MICROSCOPY; MICROSTRUCTURE; PROCESSING; RADIATION DETECTION; SCATTERING; SIZE