Published June 2010
| Version v1
Journal article
Structural characterization and dehydration kinetics of Kirka inderite mineral: Application of non-isothermal models
- 1. Yildiz Technical University, Department of Chemical Engineering, Davutpasa Campus., N.127, Esenler, Istanbul (Turkey)
Description
Coats-Redfern, Arrhenius, Ozawa, Kissinger, and Doyle non-isothermal kinetic models were used to calculate the dynamic kinetic parameters for dehydration reaction of Mg-borate mineral, inderite (Kirka - Turkey) based on thermogravimetric analysis, derivative thermogravimetric analysis and differential thermal analysis. Dehydration experiments were carried out at different heating rates of 2, 5, 10, 15, and 20 deg. C/min in a pure nitrogen atmosphere. Structural and morphological properties have been characterized by X-Ray diffraction, Fourier transform-infrared spectroscopy, Scanning electron microscopy-energy dispersive spectroscopy, and Inductively coupled plasma-optical emission spectroscopy techniques.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.matchar.2010.03.009Additional details
Identifiers
- DOI
- 10.1016/j.matchar.2010.03.009;
- PII
- S1044-5803(10)00085-9;
Publishing Information
- Journal Title
- Materials Characterization
- Journal Volume
- 61
- Journal Issue
- 6
- Journal Page Range
- p. 640-647
- ISSN
- 1044-5803
- CODEN
- MACHEX
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 44025567
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- BORATES; CRYSTAL STRUCTURE; DEHYDRATION; DIFFERENTIAL THERMAL ANALYSIS; EMISSION SPECTROSCOPY; HEATING RATE; INFRARED SPECTRA; MAGNESIUM COMPOUNDS; MINERALS; NITROGEN; SCANNING ELECTRON MICROSCOPY; TEMPERATURE DEPENDENCE; THERMAL GRAVIMETRIC ANALYSIS; X-RAY DIFFRACTION
- Descriptors DEC
- ALKALINE EARTH METAL COMPOUNDS; BORON COMPOUNDS; CHEMICAL ANALYSIS; COHERENT SCATTERING; DIFFRACTION; ELECTRON MICROSCOPY; ELEMENTS; GRAVIMETRIC ANALYSIS; MICROSCOPY; NONMETALS; OXYGEN COMPOUNDS; QUANTITATIVE CHEMICAL ANALYSIS; SCATTERING; SPECTRA; SPECTROSCOPY; THERMAL ANALYSIS
Optional Information
- Copyright
- Copyright (c) 2010 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.