Published June 2010 | Version v1
Journal article

Structural characterization and dehydration kinetics of Kirka inderite mineral: Application of non-isothermal models

  • 1. Yildiz Technical University, Department of Chemical Engineering, Davutpasa Campus., N.127, Esenler, Istanbul (Turkey)

Description

Coats-Redfern, Arrhenius, Ozawa, Kissinger, and Doyle non-isothermal kinetic models were used to calculate the dynamic kinetic parameters for dehydration reaction of Mg-borate mineral, inderite (Kirka - Turkey) based on thermogravimetric analysis, derivative thermogravimetric analysis and differential thermal analysis. Dehydration experiments were carried out at different heating rates of 2, 5, 10, 15, and 20 deg. C/min in a pure nitrogen atmosphere. Structural and morphological properties have been characterized by X-Ray diffraction, Fourier transform-infrared spectroscopy, Scanning electron microscopy-energy dispersive spectroscopy, and Inductively coupled plasma-optical emission spectroscopy techniques.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.matchar.2010.03.009

Additional details

Identifiers

DOI
10.1016/j.matchar.2010.03.009;
PII
S1044-5803(10)00085-9;

Publishing Information

Journal Title
Materials Characterization
Journal Volume
61
Journal Issue
6
Journal Page Range
p. 640-647
ISSN
1044-5803
CODEN
MACHEX

Optional Information

Copyright
Copyright (c) 2010 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.