A green synthesis of a layered titanate, potassium lithium titanate; lower temperature solid-state reaction and improved materials performance
- 1. Department of Earth Sciences, Waseda University, 1-6-1 Nishiwaseda, Shinjuku-ku, Tokyo 169-8050 (Japan)
- 2. Graduate School of Creative Science and Engineering, Waseda University, 1-6-1 Nishiwaseda, Shinjuku-ku, Tokyo 169-8050 (Japan)
Description
A layered titanate, potassium lithium titanate, with the size range from 0.1 to 30 µm was prepared to show the effects of the particle size on the materials performance. The potassium lithium titanate was prepared by solid-state reaction as reported previously, where the reaction temperature was varied. The reported temperature for the titanate preparation was higher than 800 °C, though 600 °C is good enough to obtain single-phase potassium lithium titanate. The lower temperature synthesis is cost effective and the product exhibit better performance as photocatalysts due to surface reactivity. - Graphical abstract: Finite particle of a layered titanate, potassium lithium titanate, was prepared by solid-state reaction at lower temperature to show modified materials performance. Display Omitted - Highlights: • Potassium lithium titanate was prepared by solid-state reaction. • Lower temperature reaction resulted in smaller sized particles of titanate. • 600 °C was good enough to obtain single phased potassium lithium titanate. • The product exhibited better performance as photocatalyst
Availability note (English)
Available from http://dx.doi.org/10.1016/j.jssc.2013.07.020Additional details
Identifiers
- DOI
- 10.1016/j.jssc.2013.07.020;
- PII
- S0022-4596(13)00343-5;
Publishing Information
- Journal Title
- Journal of Solid State Chemistry
- Journal Volume
- 206
- Journal Page Range
- p. 9-13
- ISSN
- 0022-4596
- CODEN
- JSSCBI
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 45095330
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Descriptors DEI
- LAYERS; LITHIUM TITANATES; PARTICLE SIZE; PARTICLES; POTASSIUM; SOLIDS; SYNTHESIS
- Descriptors DEC
- ALKALI METAL COMPOUNDS; ALKALI METALS; ELEMENTS; LITHIUM COMPOUNDS; METALS; OXYGEN COMPOUNDS; SIZE; TITANATES; TITANIUM COMPOUNDS; TRANSITION ELEMENT COMPOUNDS
Optional Information
- Copyright
- Copyright (c) 2013 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.