Published October 2013 | Version v1
Journal article

A green synthesis of a layered titanate, potassium lithium titanate; lower temperature solid-state reaction and improved materials performance

  • 1. Department of Earth Sciences, Waseda University, 1-6-1 Nishiwaseda, Shinjuku-ku, Tokyo 169-8050 (Japan)
  • 2. Graduate School of Creative Science and Engineering, Waseda University, 1-6-1 Nishiwaseda, Shinjuku-ku, Tokyo 169-8050 (Japan)

Description

A layered titanate, potassium lithium titanate, with the size range from 0.1 to 30 µm was prepared to show the effects of the particle size on the materials performance. The potassium lithium titanate was prepared by solid-state reaction as reported previously, where the reaction temperature was varied. The reported temperature for the titanate preparation was higher than 800 °C, though 600 °C is good enough to obtain single-phase potassium lithium titanate. The lower temperature synthesis is cost effective and the product exhibit better performance as photocatalysts due to surface reactivity. - Graphical abstract: Finite particle of a layered titanate, potassium lithium titanate, was prepared by solid-state reaction at lower temperature to show modified materials performance. Display Omitted - Highlights: • Potassium lithium titanate was prepared by solid-state reaction. • Lower temperature reaction resulted in smaller sized particles of titanate. • 600 °C was good enough to obtain single phased potassium lithium titanate. • The product exhibited better performance as photocatalyst

Availability note (English)

Available from http://dx.doi.org/10.1016/j.jssc.2013.07.020

Additional details

Identifiers

DOI
10.1016/j.jssc.2013.07.020;
PII
S0022-4596(13)00343-5;

Publishing Information

Journal Title
Journal of Solid State Chemistry
Journal Volume
206
Journal Page Range
p. 9-13
ISSN
0022-4596
CODEN
JSSCBI

INIS

Country of Publication
United States
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
45095330
Subject category
S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
Descriptors DEI
LAYERS; LITHIUM TITANATES; PARTICLE SIZE; PARTICLES; POTASSIUM; SOLIDS; SYNTHESIS
Descriptors DEC
ALKALI METAL COMPOUNDS; ALKALI METALS; ELEMENTS; LITHIUM COMPOUNDS; METALS; OXYGEN COMPOUNDS; SIZE; TITANATES; TITANIUM COMPOUNDS; TRANSITION ELEMENT COMPOUNDS

Optional Information

Copyright
Copyright (c) 2013 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.