Published August 1995 | Version v1
Journal article

Fracture characteristics of Czochralski-grown Y3Al5O12

  • 1. Colorado School of Mines, Golden, CO (United States). Dept. of Metallurgical and Materials Engineering
  • 2. Los Alamos National Lab., NM (United States). Materials Science and Technology Division

Description

The fracture surfaces of single-crystal Y3al5O12 (YAG) have been examined in detail using differential interference microscopy and atomic force microscopy. In YAG crystals grown in 1977 by the Czochralski method strikingly regular undulations of microscopic and submicroscopic dimensions (4--20 nm in amplitude, 1--20 microm in wavelength) are observed on every fracture surface. The undulations do not exhibit typical characteristics of Wallner lines; furthermore, they are not observed in identical fracture tests for YAG crystals grown in 1990 by the Czochralski method. Transmission electron microscopy reveals that the crystals grown in 1977 exhibit a periodic fluctuation of the ratio of the concentrations of aluminum to yttrium, suggesting that the fracture surface features are caused by periodic astoichiometry

Additional details

Publishing Information

Journal Title
Journal of the American Ceramic Society
Journal Volume
78
Journal Issue
8
Journal Page Range
p. 2282-2286.
ISSN
0002-7820
CODEN
JACTAW