Published 2011
| Version v1
Journal article
Synthesis of 3-Bromotetronamides via Amination of 3,4-Dibromofuran-2(5H)-one
- 1. Instituto Nacional de Ciencia e Tecnologia (INCT) em Energia, Salvador, BA (Brazil)
- 2. Universidade Federal da Bahia (IQ/UFBA), Salvador, BA (Brazil). Inst. de Quimica
- 3. Universidade Federal de Goias (IF/UFG), Goiania (Brazil). Inst. de Fisica
Description
This work describes the direct synthesis of 3-bromotetronamides in good yields through the reaction of 3,4-dibromofuran-2(5H)-one, obtained from furfural, with primary and secondary amines. Aromatic amines were more tolerated than aliphatic and heteroaromatic ones. The X-ray structures of five derivatives are described. (author)
Availability note (English)
Available from http://www.scielo.br/pdf/jbchs/v22n3/v22n3a26.pdfAdditional details
Identifiers
Publishing Information
- Journal Title
- Journal of the Brazilian Chemical Society
- Journal Volume
- 22
- Journal Issue
- 3
- Journal Page Range
- p. 598-603
- ISSN
- 0103-5053
- CODEN
- JOCSET
INIS
- Country of Publication
- Brazil
- Country of Input or Organization
- Brazil
- INIS RN
- 42035477
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Descriptors DEI
- AMINATION; BENZALDEHYDE; BROMINE; CARBON 13; CATALYSTS; CRYSTALLOGRAPHY; DMSO; FURANS; HEXANE; INFRARED SPECTRA; LIQUID COLUMN CHROMATOGRAPHY; MELTING POINTS; MORPHOLINES; NMR SPECTRA; PALLADIUM; X-RAY DIFFRACTION
- Descriptors DEC
- ALDEHYDES; ALKANES; AMINES; CARBON ISOTOPES; CHEMICAL REACTIONS; CHROMATOGRAPHY; COHERENT SCATTERING; DIFFRACTION; ELEMENTS; ETHERS; EVEN-ODD NUCLEI; HALOGENS; HETEROCYCLIC COMPOUNDS; HYDROCARBONS; ISOTOPES; LIGHT NUCLEI; METALS; NONMETALS; NUCLEI; ORGANIC COMPOUNDS; ORGANIC NITROGEN COMPOUNDS; ORGANIC OXYGEN COMPOUNDS; ORGANIC SULFUR COMPOUNDS; PHYSICAL PROPERTIES; PLATINUM METALS; SCATTERING; SEPARATION PROCESSES; SPECTRA; STABLE ISOTOPES; SULFOXIDES; THERMODYNAMIC PROPERTIES; TRANSITION ELEMENTS; TRANSITION TEMPERATURE