Published March 11, 2022 | Version v1
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Pitting corrosion sensitivity of AISI 316L stainless steel produced by selective laser melting and wire arc additive manufacturing

Description

Additive Layer Manufacturing (ALM) processes have been booming in recent years. They open up a whole new field of possibilities for the design of metal parts with complex geometries and multi-scale structural patterns like lattice structures. Compared to the possibilities offered by conventional, so-called subtractive processes, these technologies allow gains in cost, mass, functional performance and realization. However, the lack of knowledge on the properties and durability of the parts obtained limits their use at present. The characterization of parts made by additive manufacturing is a key point for the deployment of these technologies. Thus, more and more studies are conducted to address issues related to this production method, including the sensitivity to corrosion of metals obtained by ALM. In this study, we are interested in the AISI 316L austenitic stainless steel which is used in many fields such as chemical, pharmaceutical, oil, food and maritime industries. Its resistance to the marine and acid environment and its important ductility make it a widely used material. This is why the development of 316L stainless steel by additive manufacturing is a real issue. Two additive manufacturing technologies are studied, the first is the selective laser melting (SLM) and the second is the wire arc additive manufacturing (WAAM). The properties of the materials obtained with these manufacturing technologies are compared with those of an AISI 316L stainless steel from the conventional industry. The investigations focus on the impact of the manufacturing process and of a heat treatment aiming at erasing the thermo-mechanical transition of the part, on the microstructure of the material and the effect of this one on the sensitivity to corrosion. The coupling between the microstructure and the corrosion resistance is studied using an original approach coupling potentiostatic pulses tests and a statistical analysis of the damage to compare the sensitivity to pitting corrosion of the materials and to allow a better understanding of the damage mechanisms. (author)

Abstract (French)

Les procedes de fabrication additive (Additive Layer Manufacturing, ALM) sont en plein essor ces dernieres annees. Ils ouvrent un champ des possibles pour la conception de pieces metalliques de geometries complexes et de motifs structuraux multi-echelles (treillis ou encore structures lattices). En comparaison avec les possibilites qu'offrent les procedes conventionnels, dits soustractifs, ces technologies permettent des gains en cout, en masse, en performance fonctionnelle et en realisation. Cependant, le manque de connaissances sur les proprietes et la durabilite des pieces obtenues limite actuellement leurs utilisations. La caracterisation des pieces realisees par fabrication additive est alors un point cle pour le deploiement de ces technologies. Ainsi, de plus en plus d'etudes, sont realisees afin de repondre aux problematiques liees a cette methode de production, notamment la sensibilite a la corrosion des metaux obtenus par ALM. Dans cette etude, on s'interesse a l'acier inoxydable austenitique AISI 316L qui est utilise dans de nombreux domaines tels que les industries chimiques, pharmaceutiques, petrolieres, agro-alimentaires et maritimes. Sa resistance au milieu marin, acide et son importante ductilite en font un materiau tres utilise. C'est pour cela que l'elaboration d'acier inoxydable 316L par fabrication additive est un enjeu reel. Deux technologies de fabrication additive sont etudiees, la premiere est la fusion selective sur lit de poudre (Selective Laser Melting, SLM) et la seconde est le depot de fil (Wire Arc Additive Manufacturing, WAAM). Les proprietes des materiaux obtenus avec ces technologies de fabrication sont comparees avec ceux d'un acier inoxydable AISI 316L issu de l'industrie conventionnelle. Les investigations portent sur l'impact du procede de fabrication et d'un traitement thermique aillant pour objectif d'effacer le passer thermo-mecanique de la piece, sur la microstructure du materiau et l'effet de celle-ci sur la sensibilite a la corrosion. Le couplage entre la microstructure et la resistance a la corrosion est etudie a l'aide d'une approche originale couplant des tests de saut de potentiel et une analyse statistique de l'endommagement pour comparer la sensibilite a la corrosion par piqure des materiaux et permettre une meilleure comprehension des mecanismes d'endommagement

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Additional details

Additional titles

Original title (French)
Sensibilite a la corrosion par piqures de l'acier inoxydable AISI 316L elabore par fusion sur lit de poudre et depot de fil

Publishing Information

Imprint Pagination
210 p.
Report number
FRCEA-TH--17067

Optional Information

Notes
187 refs.; Available from the INIS Liaison Officer for France, see the INIS website for current contact and E-mail addresses