An oxides-hydrothermal approach from bulky V2O5 powder to V3O7.H2O nanoribbons or V3O7 nanoflowers in various ethanol/water mixed solvent
Creators
- 1. College of Science, University of Shanghai for Science and Technology, Shanghai 200093 (China)
- 2. Department of Chemistry, Tongji University, Shanghai 200092 (China)
Description
V3O7.H2O nanoribbons and V3O7 nanoflowers are firstly obtained via facile oxides-hydrothermal (O-HT) route. V2O5 bulk-phase powder is directly used as precursor. The 1:1 ethanol/water and absolute ethanol are made as solvent for obtaining nanomaterials of vanadium oxides with different morphologies and structures. Characterizations of the samples are carried out using XRD, TG, FTIR, Raman-Spectra, SEM, TEM, HRTEM, SAED, and UV-vis. The large-scale fine ribbon-like V3O7.H2O nanobelts with thickness ca. 20 nm and length ca. 20-40 μm are obtained in 1:1 (v/v) ethanol/water mixed solvent. The V3O7 nanoflowers are constructed by numerous whisker-like nanocrystal or petal-like are obtained in absolute ethanol solvent with the thickness about 20 nm and the size ca. 2-3 μm. The formation mechanism of the sample is discussed
Availability note (English)
Available from http://dx.doi.org/10.1016/j.materresbull.2008.09.045Additional details
Identifiers
- DOI
- 10.1016/j.materresbull.2008.09.045;
- PII
- S0025-5408(08)00343-7;
Publishing Information
- Journal Title
- Materials Research Bulletin
- Journal Volume
- 44
- Journal Issue
- 5
- Journal Page Range
- p. 1142-1147
- ISSN
- 0025-5408
- CODEN
- MRBUAC
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 40069805
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- CRYSTAL GROWTH; ELECTRON DIFFRACTION; ETHANOL; FOURIER TRANSFORMATION; INFRARED SPECTRA; LENGTH; MIXED SOLVENTS; MORPHOLOGY; NANOSTRUCTURES; RAMAN SPECTRA; SCANNING ELECTRON MICROSCOPY; TRANSMISSION ELECTRON MICROSCOPY; VANADIUM OXIDES; X-RAY DIFFRACTION
- Descriptors DEC
- ALCOHOLS; CHALCOGENIDES; COHERENT SCATTERING; DIFFRACTION; DIMENSIONS; DISPERSIONS; ELECTRON MICROSCOPY; HYDROXY COMPOUNDS; INTEGRAL TRANSFORMATIONS; MICROSCOPY; MIXTURES; ORGANIC COMPOUNDS; OXIDES; OXYGEN COMPOUNDS; SCATTERING; SOLVENTS; SPECTRA; TRANSFORMATIONS; TRANSITION ELEMENT COMPOUNDS; VANADIUM COMPOUNDS
Optional Information
- Copyright
- Copyright (c) 2008 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.