Effect of sintering temperature on Structural and Dielectric properties of Sn substituted CuFe2O4 Nanoparticles
- 1. Department of Physics, Government College of Technology, Coimbatore, Tamilnadu-13 (India)
- 2. Department of Physics, Dr. NGP Institute of Technology, Coimbatore, Tamil Nadu-48 (India)
- 3. Department of Physics, Sri Ramakrishna Mission Vidyalaya College of Arts & Science, Coimbatore, Tamilnadu-20 (India)
Description
Sn substituted Cu ferrite nanoparticles were synthesized (x=0.04, 0.06) by chemical co-precipitation method. The prepared samples were sintered at 300 °C, 600 °C, 900 °C. From XRD analyses the particle size increased due to sintering temperature. The lattice parameter decreased while increasing the concentration of Sn elements and sintering temperature. From SAED pattern of TEM results, the superimposition of bright spots confirms the polycrystalline nature. FT-IR results show the octahedral and tetrahedral stretching sites respectively. The remarkable change of dielectric constant and loss was found to be in the range of 100 KHZ- 700 MHZ. - Highlights: • The lattice parameter decreased while increasing the concentration of Sn doping. • The average particle size is in the range of 25–50 nm. • The SAED pattern confirms the polycrystalline nature.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.jmmm.2016.09.077Additional details
Identifiers
- DOI
- 10.1016/j.jmmm.2016.09.077;
- PII
- S0304-8853(16)31671-7;
Publishing Information
- Journal Title
- Journal of Magnetism and Magnetic Materials
- Journal Volume
- 423
- Journal Page Range
- p. 250-255
- ISSN
- 0304-8853
- CODEN
- JMMMDC
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 48102261
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- CONCENTRATION RATIO; COPPER COMPOUNDS; COPRECIPITATION; DIELECTRIC MATERIALS; FERRITE; FOURIER TRANSFORM SPECTROMETERS; INFRARED SPECTRA; KHZ RANGE; LATTICE PARAMETERS; MHZ RANGE; NANOPARTICLES; PARTICLE SIZE; PERMITTIVITY; POLYCRYSTALS; SINTERING; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION
- Descriptors DEC
- ALLOYS; CARBON ADDITIONS; COHERENT SCATTERING; CRYSTALS; DIELECTRIC PROPERTIES; DIFFRACTION; DIMENSIONLESS NUMBERS; ELECTRICAL PROPERTIES; ELECTRON MICROSCOPY; FABRICATION; FREQUENCY RANGE; IRON ALLOYS; MATERIALS; MEASURING INSTRUMENTS; MICROSCOPY; PARTICLES; PHYSICAL PROPERTIES; PRECIPITATION; SCATTERING; SEPARATION PROCESSES; SIZE; SPECTRA; SPECTROMETERS; TRANSITION ELEMENT ALLOYS; TRANSITION ELEMENT COMPOUNDS
Optional Information
- Copyright
- Copyright (c) 2016 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.