Published December 2008 | Version v1
Journal article Metadata-only

New 12-tungstophosphate-based organic-inorganic hybrid synthesis, spectroscopic characterization, x-ray determination and thermal behavior

Creators

  • 1. Tarbiat Modares University, Department of Chemistry, Tehran (Iran, Islamic Republic of)
  • 2. Imam Khomeini International University, Faculty of Science, Department of Chemistry, Qazvin (Iran, Islamic Republic of)

Description

12-Tungstophosphate-based organic/inorganic hybrid, [HNMPA]3[O40PW12].0.5NMPA.2H2O (NMPA = N-methylpropionamide) was synthesized and characterized by IR, UV-Vis, 1H, 13C and 31P NMR spectroscopies, elemental analysis, thermal gravimetric analysis, differential thermal analysis and single crystal X-ray determination. Full decomposition of the hybrid leads to WO3 powder was studied by IR, scanning electron microscopy and XRD

Availability note (English)

Available from Atomic Energy Organization of Iran

Additional details

Publishing Information

Journal Title
Journal of the Iranian Chemical Society (Print)
Journal Volume
5
Journal Issue
no.4
Journal Page Range
p. 588-594
ISSN
1735-207X

INIS

Country of Publication
Iran, Islamic Republic of
Country of Input or Organization
Iran, Islamic Republic of
INIS RN
40043656
Subject category
S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
Descriptors DEI
CRYSTAL STRUCTURE; DECOMPOSITION; DIFFERENTIAL THERMAL ANALYSIS; HYBRIDIZATION; INORGANIC POLYMERS; NMR SPECTROMETERS; ORGANIC COMPOUNDS; SCANNING ELECTRON MICROSCOPY; SYNTHESIS; THERMAL GRAVIMETRIC ANALYSIS; TUNGSTOPHOSPHATES; ULTRASONIC WAVES; X-RAY SPECTROSCOPY
Descriptors DEC
CHEMICAL ANALYSIS; CHEMICAL REACTIONS; ELECTRON MICROSCOPY; GRAVIMETRIC ANALYSIS; MEASURING INSTRUMENTS; MICROSCOPY; OXYGEN COMPOUNDS; PHOSPHORUS COMPOUNDS; POLYMERS; QUANTITATIVE CHEMICAL ANALYSIS; REFRACTORY METAL COMPOUNDS; SOUND WAVES; SPECTROMETERS; SPECTROSCOPY; THERMAL ANALYSIS; TRANSITION ELEMENT COMPOUNDS; TUNGSTEN COMPOUNDS