Published 1987 | Version v1
Book

Nitridation of titanium and zirconium powders mixed with ammonium chloride under high temperature-high pressure ammonia

  • 1. Tokyo Inst. of Tech., Yokohama

Description

Nitridation of Ti and Zr metal powders mixed with or without NH4Cl under high temperature and high-pressure ammonia was investigated. Without NH4Cl, only hydrides of Ti or Zr appeared under experimental conditions; with NH4Cl, TiN and ZrN appeared above 5000 and 6000C, respectively, even under 0.1 MPa NH3. Crystallite sizes for TiN and ZrN were 8 to 9 nm and 12 nm by X ray. Lattice parameters of TiN were 0.4232 to 0.4236 nm (corresponding to N/Ti = 0.80 to 1.05), and of ZrN were 0.4559 to 0.4566 (corresponding to N/Zr = 1.25 to 1.30)

Additional details

Publishing Information

Publisher
American Ceramic Society Inc.
Imprint Place
Westerville, OK (USA)
ISBN
0-916094-83-9
Imprint Title
Ceramic powder science
Imprint Pagination
823 p.
Series
Advances in ceramics: Volume 21.
Journal Page Range
p. 279-288.

Conference

Title
synthesis, processing, and characterization conference.
Acronym
Ceramic powder science and technology
Dates
3-6 Aug 1986.
Place
Boston, MA (USA).

Optional Information

Secondary number(s)
CONF-860883--.