Published January 1990 | Version v1
Journal article Metadata-only

Amorphous Bi2Pb0.6Sr2Ca2Cu3Ox obtained by melt-spinning and its superconductivity after crystallisation

Creators

  • 1. Institut National Polytechnique, 38 - Grenoble (France)
  • 2. Centre National de la Recherche Scientifique, 38 - Grenoble (France). Centre de Recherches sur les Tres Basses Temperatures

Description

Previous quenching experiments on 2212 bismuth containing high Tc oxides have been extended to the 2223 compound with lead addition. Amorphous Bi2Pb0.6Sr2Ca2Cu3Ox was prepared by a modified melt-spinning technique and samples in the form of small tapes and wires were obtained. The subsequent evolution of the amorphous oxide during annealing was monitored by differential scanning calorimetry (DSC). The glass transition was found to occur at Tg = 680 K and the onset of crystallisation at T = 730 K. After oxygen annealing, magnetic susceptibility measurements showed evidence of two superconducting phases with transition temperatures at Tc = 110 K and Tc = 75 K respectively

Additional details

Publishing Information

Journal Title
Revue de Physique Appliquee
Journal Volume
25
Journal Issue
1
Series
Rev. Phys. Appl.
Journal Page Range
9-12
ISSN
0035-1687
CODEN
RPHAA

INIS

Country of Publication
France
Country of Input or Organization
France
INIS RN
21052446
Subject category
S36: MATERIALS SCIENCE; S36: MATERIALS SCIENCE; S36: MATERIALS SCIENCE;
Descriptors DEI
AMORPHOUS STATE; ANNEALING; BISMUTH OXIDES; CALCIUM OXIDES; COPPER OXIDES; CRYSTALLIZATION; LEAD OXIDES; MAGNETIC SUSCEPTIBILITY; STRONTIUM OXIDES; SUPERCONDUCTIVITY; SYNTHESIS; TRANSITION TEMPERATURE
Descriptors DEC
ALKALINE EARTH METAL COMPOUNDS; BISMUTH COMPOUNDS; CALCIUM COMPOUNDS; CHALCOGENIDES; COPPER COMPOUNDS; ELECTRIC CONDUCTIVITY; ELECTRICAL PROPERTIES; HEAT TREATMENTS; LEAD COMPOUNDS; MAGNETIC PROPERTIES; OXIDES; OXYGEN COMPOUNDS; PHASE TRANSFORMATIONS; PHYSICAL PROPERTIES; STRONTIUM COMPOUNDS; THERMODYNAMIC PROPERTIES; TRANSITION ELEMENT COMPOUNDS