Complementary study of molecular dynamics and domain sizes in heterogenous nanocomposites PBT/DA-C60 and PBT/TCNEO-C60
Creators
- 1. High Pressure Physics Division, Department of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan (Poland)
- 2. Polymer Processing Division, Institute of Materials Technology, Poznań University of Technology, Piotrowo 3, 61-138 Poznan (Poland)
- 3. Laboratory of Microbiocides Chemistry, Department of Chemistry, Adam Mickiewicz University, Grunwaldzka 6, 60-780 Poznan (Poland)
- 4. Department of Chemistry, Jagiellonian University, Ingardena Street 9, Krakow (Poland)
Description
A comprehensive study of molecular dynamics and structure in new heterogenous nanocomposites based on poly(butylene terephthalate) and nanoparticles C60 modified by n-decylamine or tetracyanoethylene oxide has been performed. The domain structure of new nanocomposites has been investigated by Fourier transform infrared spectroscopy, wide-angle X-ray scattering, and differential scanning calorimetry techniques. Solid-state 1H NMR techniques were used to study molecular dynamics and domain sizes in new nanocomposites. Information about the electronic properties of these nanocomposites was obtained by means of electron paramagnetic resonance method. It was shown that the structure and molecular dynamics of new nanocomposites were strongly dependent on the properties and concentration of fullerene derivates.
Additional details
Identifiers
- DOI
- 10.1063/1.4880297;
Publishing Information
- Journal Title
- Journal of Applied Physics
- Journal Volume
- 115
- Journal Issue
- 20
- Journal Page Range
- p. 204914-204914.10
- ISSN
- 0021-8979
- CODEN
- JAPIAU
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 46010459
- Subject category
- S77: NANOSCIENCE AND NANOTECHNOLOGY;
- Descriptors DEI
- CALORIMETRY; COMPOSITE MATERIALS; DOMAIN STRUCTURE; ELECTRON SPIN RESONANCE; FOURIER TRANSFORM SPECTROMETERS; FULLERENES; HYDROGEN 1; MOLECULAR DYNAMICS METHOD; NANOPARTICLES; NANOSTRUCTURES; NUCLEAR MAGNETIC RESONANCE; SOLIDS; X-RAY DIFFRACTION
- Descriptors DEC
- CALCULATION METHODS; CARBON; COHERENT SCATTERING; DIFFRACTION; ELEMENTS; HYDROGEN ISOTOPES; ISOTOPES; LIGHT NUCLEI; MAGNETIC RESONANCE; MATERIALS; MEASURING INSTRUMENTS; NONMETALS; NUCLEI; ODD-EVEN NUCLEI; PARTICLES; RESONANCE; SCATTERING; SPECTROMETERS; STABLE ISOTOPES
Optional Information
- Notes
- (c) 2014 AIP Publishing LLC