Published 2020
| Version v1
Book
Thermal, spectroscopic and reversible hydration studies of Tetraaquabis (4-Nitrobenzoato) manganese(II) Dihydrate
Creators
- 1. Department of Chemistry, Govt. College of Arts, Science and Commerce, Sanquelim, Goa (India)
Description
Tetraaquabis(4-nitrobenzoato)Manganese(II) dihydrate, (Mn(H2O)4(4-nba)2).2H2O1 complex has been synthesized by reacting freshly precipitated MnCO3 obtained from the reaction of MnCl2.4H2O and the sodium carbonate, with 4-nitrobenzoic acid (4-nbaH) in water. The complex 1 is dehydrated to (Mn((4-nba)2) 2 on heating at 180°C and can be reversibly hydrated as evidenced by IR spectra and isothermal weight loss studies. The compounds are characterized by elemental analysis, infrared spectra, X-ray powder pattern and thermal studies. Based on elemental analysis and gravimetric analysis of 4-nbaH, complexes were formulated. At 450°C, the compounds can be pyrolysed to cubic Mn2O3. (author)
Additional details
Publishing Information
- Publisher
- Bhabha Atomic Research Centre
- Imprint Place
- Mumbai (India)
- Imprint Title
- Proceedings of the twenty second DAE-BRNS symposium on thermal analysis - thermal techniques for advanced materials: book of abstracts
- Imprint Pagination
- 322 p.
- Journal Page Range
- p. 241-243
Conference
- Title
- 22. DAE-BRNS symposium on thermal analysis - thermal techniques for advanced materials
- Acronym
- THERMANS-2020
- Dates
- 30 Jan - 1 Feb 2020
- Place
- Mumbai (India)
INIS
- Country of Publication
- India
- Country of Input or Organization
- India
- INIS RN
- 51088476
- Subject category
- S36: MATERIALS SCIENCE;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- HYDRATION; MAGNESIUM COMPOUNDS; SPECTROSCOPY; THERMODYNAMIC PROPERTIES; X-RAY DIFFRACTION
- Descriptors DEC
- ALKALINE EARTH METAL COMPOUNDS; COHERENT SCATTERING; DIFFRACTION; PHYSICAL PROPERTIES; SCATTERING; SOLVATION