Published January 5, 1976 | Version v1
Journal article

The crystal structure of K3[(UO2)3F9-H2O)]-2H2O

  • 1. Ecole Centrale des Arts et Manufactures, 92 - Chatenay-Malabry (France). Inst. de Chimie

Description

K3[(UO2)3F9-H2O]-2H2O crystallizes in the orthorhombic system, space group Pmcn: a=12.686(1); b=10.444(1); c=12.877(1)A; Z=4; dsub(th)=4.456. The crystal structure has been determined by Patterson and Fourier methods and refined by least-square calculations to R=0.063 for 2785 reflexions. The structure is composed of K+ ions, water molecules and sheets of complex anions with a trinuclear group of formula [(UO2)3-H2O-F7-Fsub(4/2)]sub(infinity)sup(3-)

Abstract (French)

Le compose K3[(UO2)3F9-H2O]-2H2O cristallise dans le systeme orthorhombique de groupe spacial Pmcn: a=12,686(1); b=10,444(1); c=12,877(1)A; Z=4; dsub(th)=4,456. L'affinement de 2785 reflexions a conduit a un facteur R de 6,3%. La structure est composee d'ions K+, de molecules d'eau et de feuillets d'anions complexes ayant comme motif de base un groupement trinucleaire [(UO2)3-H2O-F7-Fsub(4/2)]sub(infinity)sup(3-)

Additional details

Additional titles

Original title (French)
Structure cristalline du compose K

Publishing Information

Journal Title
C. R., Ser. C
Journal Volume
282
Journal Issue
1) p+ 49-51
Series
C. R., Ser. C.

INIS