Published April 2019 | Version v1
Journal article

Mapping the full lattice strain tensor of a single dislocation by high angular resolution transmission Kikuchi diffraction (HR-TKD)

  • 1. Department of Engineering Science, University of Oxford, Parks Road, Oxford OX1 3PJ (United Kingdom)
  • 2. Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH (United Kingdom)

Description

The full lattice strain tensor and lattice rotations induced by a dislocation in pure tungsten were mapped using high-resolution transmission Kikuchi diffraction (HR-TKD) in a SEM. The HR-TKD measurement agrees very well with a forward calculation using an elastically isotropic model of the dislocation and its Burgers vector. Our results demonstrate that the spatial and angular resolution of HR-TKD in SEM is sufficiently high to resolve the details of lattice distortions near individual dislocations. This capability opens a number of new interesting opportunities, for example determining the Burgers vector of an unknown dislocation in a fast and straightforward way.

Additional details

Identifiers

DOI
10.1016/j.scriptamat.2018.12.039;
PII
S1359646219300302;

Publishing Information

Journal Title
Scripta Materialia
Journal Volume
164
Journal Page Range
p. 36-41
ISSN
1359-6462
CODEN
SCMAF7

INIS

Country of Publication
United Kingdom
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
55043101
Subject category
S36: MATERIALS SCIENCE;
Descriptors DEI
BACKSCATTERING; BURGERS VECTOR; DISLOCATIONS; ELECTRON DIFFRACTION; MAPPING; RESOLUTION; ROTATION; SCANNING ELECTRON MICROSCOPY; TENSORS; TUNGSTEN
Descriptors DEC
COHERENT SCATTERING; CRYSTAL DEFECTS; CRYSTAL STRUCTURE; DIFFRACTION; ELECTRON MICROSCOPY; ELEMENTS; LINE DEFECTS; METALS; MICROSCOPY; MOTION; REFRACTORY METALS; SCATTERING; TRANSITION ELEMENTS

Optional Information

Copyright
Copyright (c) 2019 The Authors. Published by Elsevier Ltd on behalf of Acta Materialia Inc.