Published 1990 | Version v1
Miscellaneous Open

Iron (III) oxides solvothermal synthesis. The effect of acetate group

  • 1. UNESP, Araraquara, SP (Brazil). Dept. de Fisico-Quimica

Description

Iron oxydes preparation have been extensively studied due to large application of these materials. In this work it was utilized the precipitation method together with solvothermal process to prepare iron oxyde. It was studied the system iron (III) nitrate hydrolised with aqueous amonia, in 2-propanol, in presence of acetate group. Final product, where sodium acetate was used as acetate group precursor, showed goethite and hematite formation while when acetic acid was the precursor, it was not observed any crystalline fase iron oxyde. The product was characterized by X-ray diffraction and vibrational spectroscopy. (author)

Abstract (Portuguese)

A preparacao de oxidos de ferro tem sido extensamente estudada devido a ampla aplicacao destes materiais. Neste trabalho, utilizou-se o metodo de precipitacao associado ao processo solvotermico para preparar oxido de ferro. Estudou-se nitrato ferrico hidrolisado com amonia aquosa em isopropanol, na presenca do grupo acetato. O produto obtido, no qual acetato de sodio foi o precursor do grupo acetato, mostrou a formacao de goethita e de hematita, enquanto que, quando acido acetico foi o precursor, nao houve formacao de oxido de ferro cristalino. O produto foi caracterizado por difratometria de raio-X e espectroscopia vibracional. (autor)

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Additional details

Additional titles

Original title (Portuguese)
Sintese solvotermica de oxido de ferro. O efeito do grupo acetato

Publishing Information

Imprint Title
Proceedings of the 34. Brazilian Congress on Ceramics. v. 1
Imprint Pagination
341 p.
Journal Page Range
p. 258-264.
Report number
INIS-BR--2255

Conference

Title
34. Brazilian Congress on Ceramics.
Dates
20-23 May 1990.
Place
Blumenau, SC (Brazil).

Optional Information

Notes
Imprint:Anais do 34. Congresso Brasileiro de Ceramica. v. 1.