Published June 15, 1987 | Version v1
Journal article

The monoclinic perovskites Sr2CaUO6 and Ba2SrUO6. A Rietveld refinement of neutron powder diffraction data

  • 1. Rijksuniversiteit Leiden (Netherlands). Gorlaeus Labs.

Description

Sr2CaUO6, Mr=549.35, monoclinic, P21/n. At T=295 K, a=5.9377(2), b=6.0734(2), c=8.4563(3) A, β=90.14(1)0, V=304.95(3) A3, Z=2, Dx=5.983(1) Mg m-3, μR=0.12 [λ=2.5791(4) A, Rwp=6.36%]. Ba2SrUO6, Mr=696.33, monoclinic, P21/n. At T=295 K, a=6.2501(4), b=6.2697(4), c=8.8355(6) A, β=89.760(8)0, V=346.22(2) A3, Z=2, Dx=6.680(1) Mg m-3, μR=0.17 [λ=2.5791(4) A, Rwp=6.40%]. The structures have been refined by Rietveld analysis of neutron powder diffraction data recorded at room temperature for 147 (Sr2CaUO6) and 168 (Ba2SrUO6) reflections. The structures are of a monoclinic GdFeO3-type perovskite. The octahedra ions are in complete order. (orig.)

Additional details

Publishing Information

Journal Title
Acta Crystallogr., Sect. C
Journal Volume
43
Journal Issue
6
Series
Acta Crystallogr., Sect. C.
Journal Page Range
1033-1036
ISSN
0108-2701
CODEN
ACSCE