Published 1989
| Version v1
Report
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Determination of non-metallic elements in actinide complexes by oxygen flask combustion (OFC): chlorine and fluorine
Creators
- 1. Bhabha Atomic Research Centre, Bombay (India). Radiochemistry Div.
Description
The oxygen flask combustion followed by ion selective electrode measurement has been found to be the most suitable from the point of view of elegance and simplicity for the determination of chlorine and fluorine in actinide complexes. The method has been found to be particularly suitable for glove box adaptation. This report describes the determination of chlorine and fluorine in several uranium complexes, some plutonium complexes and organic analytical standards by this method. The precision and accuracy of the measurements in the milligram level has been found to be quite satisfactory. (author). 16 refs., 11 tabs
Availability note (English)
MF available from INIS under the Report Number.Files
21077993.pdf
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Additional details
Publishing Information
- Imprint Pagination
- 19 p.
- Report number
- BARC--1484
INIS
- Country of Publication
- India
- Country of Input or Organization
- India
- INIS RN
- 21077993
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Is Lead record
- Yes
- Descriptors DEI
- ACCURACY; CHLORINE; COMBUSTION; FLUORINE; GLOVEBOXES; ION SELECTIVE ELECTRODE ANALYS; ORGANIC ACIDS; ORGANIC CHLORINE COMPOUNDS; ORGANIC FLUORINE COMPOUNDS; OXYGEN; PLUTONIUM COMPLEXES; SENSITIVITY; URANIUM COMPLEXES
- Descriptors DEC
- ACTINIDE COMPLEXES; CHEMICAL ANALYSIS; CHEMICAL REACTIONS; COMPLEXES; ELEMENTS; EQUIPMENT; HALOGENS; LABORATORY EQUIPMENT; NONMETALS; ORGANIC COMPOUNDS; ORGANIC HALOGEN COMPOUNDS; OXIDATION; TRANSURANIUM COMPLEXES