Published 2013 | Version v1
Journal article Metadata-only

Synthesis route and structural properties of nanoferrites

Creators

  • 1. Institute of Catalysis, Bulgarian Academy of Sciences, Sofia (Bulgaria)

Description

The nano dimensional magnesium ferrite materials Mg0.25Fe2.75O4 , Mg0.5Fe2.5O4 and MgFe2O4 with different stoichiometry were prepared by co-precipitation procedure using MgCl2 •6H2O, FeCl2 •4H2O and FeCl3 •6H2O and NaOH as precipitant. The physicochemical methods - X-ray diffraction analysis, Moessbauer spectroscopy and FTIR spectroscopy were performed to investigate the structural properties of obtained nano size magnesium ferrite type samples. The registered experimental data were determined the presence of spinel ferrites and additional precursor phases as iron oxihydroxides and double layered hydroxides in ferrite materials MgxFe3-xO4 (x=0.5;1). In the case of magnesium ferrite sample MgxFe3-xO4 (x=0.25) the existence of non-stoichiometric spinel ferrite and intermediate phase - iron oxihydroxides were observed only. Key words: magnesium ferrites, co-precipitation, physicochemical methods

Availability note (English)

Available http://www.scientific-publications.net/download/materials-methods-and-technologies-2013-1.pdf

Additional details

Identifiers

URL
http://www.scientific-publications.net/download/materials-methods-and-technologies-2013-1.pdf;

Publishing Information

Journal Title
Materials, methods and technologies (CD-ROM)
Journal Volume
7
Journal Issue
1
Journal Page Range
p. 329-336
ISSN
1313-2539

INIS

Country of Publication
Bulgaria
Country of Input or Organization
Bulgaria
INIS RN
45107988
Subject category
S77: NANOSCIENCE AND NANOTECHNOLOGY;
Descriptors DEI
COPRECIPITATION; FERRITES; FOURIER TRANSFORMATION; INFRARED SPECTRA; IRON; IRON CHLORIDES; MAGNESIUM; MAGNESIUM CHLORIDES; MOESSBAUER EFFECT; SODIUM HYDROXIDES; SPINELS; STOICHIOMETRY; SYNTHESIS; X-RAY DIFFRACTION
Descriptors DEC
ALKALI METAL COMPOUNDS; ALKALINE EARTH METAL COMPOUNDS; ALKALINE EARTH METALS; CHLORIDES; CHLORINE COMPOUNDS; COHERENT SCATTERING; DIFFRACTION; ELEMENTS; FERRIMAGNETIC MATERIALS; HALIDES; HALOGEN COMPOUNDS; HYDROGEN COMPOUNDS; HYDROXIDES; INTEGRAL TRANSFORMATIONS; IODIDES; IODINE COMPOUNDS; IRON COMPOUNDS; IRON HALIDES; IRON IODIDES; MAGNESIUM COMPOUNDS; MAGNESIUM HALIDES; MAGNETIC MATERIALS; MATERIALS; METALS; MINERALS; OXIDE MINERALS; OXYGEN COMPOUNDS; PRECIPITATION; SCATTERING; SEPARATION PROCESSES; SODIUM COMPOUNDS; SPECTRA; TRANSFORMATIONS; TRANSITION ELEMENT COMPOUNDS; TRANSITION ELEMENTS

Optional Information

Notes
19 refs., 3 figs., 1 tab.