Published November 2016
| Version v1
Journal article
Determination of 107Pd in radwaste using Ni ®Resin
- 1. Comenius University, Bratislava (Slovakia). Department of Nuclear Chemistry, Faculty of Natural Sciences
Description
A simple separation method for determination of 107Pd employing Ni ®Resin was established. Suitable conditions for Pd separation were tested. Palladium was adsorbed on Ni ®Resin from 0.5 mol L-1 HCl and eluted with 8 mol L-1 HNO3 with recoveries higher than 70 % determined by atomic absorption spectrometry. The method was applied for analysis of evaporator concentrate and radioactive sludge samples from nuclear power plants in Slovak Republic. In all analyzed samples were activity concentrations of 107Pd below minimum detectable activity. 107Pd was measured on liquid scintillation counter (TRICARB 2900/TR) using Ultima Gold AB scintillation cocktail. (author)
Additional details
Publishing Information
- Journal Title
- Journal of Radioanalytical and Nuclear Chemistry
- Journal Volume
- 310
- Journal Issue
- 2
- Journal Page Range
- p. 645-650
- ISSN
- 0236-5731
- CODEN
- JRNCDM
INIS
- Country of Publication
- Hungary
- Country of Input or Organization
- Hungary
- INIS RN
- 47125840
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Descriptors DEI
- ABSORPTION SPECTROSCOPY; ACTIVITY METERS; NITROGEN; NUCLEAR POWER PLANTS; PALLADIUM 107; RESINITE; RESINS; SEPARATION PROCESSES; SLOVAKIA
- Descriptors DEC
- BETA DECAY RADIOISOTOPES; BETA-MINUS DECAY RADIOISOTOPES; DEVELOPING COUNTRIES; EASTERN EUROPE; ELEMENTS; EUROPE; EVEN-ODD NUCLEI; INTERMEDIATE MASS NUCLEI; ISOMERIC TRANSITION ISOTOPES; ISOTOPES; MACERALS; MEASURING INSTRUMENTS; METERS; NONMETALS; NUCLEAR FACILITIES; NUCLEI; ORGANIC COMPOUNDS; ORGANIC POLYMERS; PALLADIUM ISOTOPES; PETROCHEMICALS; PETROLEUM PRODUCTS; POLYMERS; POWER PLANTS; RADIOISOTOPES; SECONDS LIVING RADIOISOTOPES; SPECTROSCOPY; THERMAL POWER PLANTS; YEARS LIVING RADIOISOTOPES
Optional Information
- Notes
- 8 refs.