Published July 2011 | Version v1
Journal article

Grain-resolved elastic strains in deformed copper measured by three-dimensional X-ray diffraction

  • 1. Center for Fundamental Research: Metal Structures in Four Dimensions, Materials Research Division, Riso DTU, Frederiksborgvej 399, DK-4000 Roskilde (Denmark)
  • 2. European Synchrotron Research Facility, 38043 Grenoble (France)
  • 3. Max-Planck-Institut fuer Eisenforschung GmbH, Max-Planck-Str. 1, 40237 Duesseldorf (Germany)
  • 4. Technische Universitaet Berlin, Sekr. BH18, Ernst-Reuter-Platz 1, 10587 Berlin (Germany)

Description

This X-ray diffraction study reports the grain-resolved elastic strains in about 1000 randomly oriented grains embedded in a polycrystalline copper sample. Diffraction data were collected in situ in the undeformed state and at a plastic strain of 1.5% while the sample was under tensile load. For each grain the centre-of-mass position was determined with an accuracy of 10 μm, the volume with a relative error of 20%, the orientation to 0.05o and the axial strain to 10-4. The elastic strain along the tensile direction exhibited a grain orientation dependence with grains within 20 deg. of <100> carrying the largest strain. While the width of the strain distribution for all grains did not change upon plastic loading, the grain-resolved data show a significant widening of the distribution evaluated for small subsets of initially elastically similar grains. This widening appears independent of the grain orientation. - Research Highlights: → X-ray diffraction study of ∼ 1000 Cu grains during in situ plastic deformation. → Grain averaged positions, orientations, volumes and elastic strain tensors derived. → Both lattice rotation and axial strain depend on the initial grain orientation. → Grains within 20o of <100> carry the largest elastic strain along the tensile axis. → The results enable evaluation and development of polycrystal plasticity models.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.matchar.2011.04.020

Additional details

Identifiers

DOI
10.1016/j.matchar.2011.04.020;
PII
S1044-5803(11)00104-5;

Publishing Information

Journal Title
Materials Characterization
Journal Volume
62
Journal Issue
7
Journal Page Range
p. 651-660
ISSN
1044-5803
CODEN
MACHEX

Optional Information

Copyright
Copyright (c) 2011 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.