Grain-resolved elastic strains in deformed copper measured by three-dimensional X-ray diffraction
Creators
- 1. Center for Fundamental Research: Metal Structures in Four Dimensions, Materials Research Division, Riso DTU, Frederiksborgvej 399, DK-4000 Roskilde (Denmark)
- 2. European Synchrotron Research Facility, 38043 Grenoble (France)
- 3. Max-Planck-Institut fuer Eisenforschung GmbH, Max-Planck-Str. 1, 40237 Duesseldorf (Germany)
- 4. Technische Universitaet Berlin, Sekr. BH18, Ernst-Reuter-Platz 1, 10587 Berlin (Germany)
Description
This X-ray diffraction study reports the grain-resolved elastic strains in about 1000 randomly oriented grains embedded in a polycrystalline copper sample. Diffraction data were collected in situ in the undeformed state and at a plastic strain of 1.5% while the sample was under tensile load. For each grain the centre-of-mass position was determined with an accuracy of 10 μm, the volume with a relative error of 20%, the orientation to 0.05o and the axial strain to 10-4. The elastic strain along the tensile direction exhibited a grain orientation dependence with grains within 20 deg. of <100> carrying the largest strain. While the width of the strain distribution for all grains did not change upon plastic loading, the grain-resolved data show a significant widening of the distribution evaluated for small subsets of initially elastically similar grains. This widening appears independent of the grain orientation. - Research Highlights: → X-ray diffraction study of ∼ 1000 Cu grains during in situ plastic deformation. → Grain averaged positions, orientations, volumes and elastic strain tensors derived. → Both lattice rotation and axial strain depend on the initial grain orientation. → Grains within 20o of <100> carry the largest elastic strain along the tensile axis. → The results enable evaluation and development of polycrystal plasticity models.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.matchar.2011.04.020Additional details
Identifiers
- DOI
- 10.1016/j.matchar.2011.04.020;
- PII
- S1044-5803(11)00104-5;
Publishing Information
- Journal Title
- Materials Characterization
- Journal Volume
- 62
- Journal Issue
- 7
- Journal Page Range
- p. 651-660
- ISSN
- 1044-5803
- CODEN
- MACHEX
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 44025690
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- COPPER; DEFORMATION; ELASTICITY; GRAIN ORIENTATION; LOADING; PLASTICITY; POLYCRYSTALS; STRAINS; SYNCHROTRON RADIATION; X-RAY DIFFRACTION
- Descriptors DEC
- BREMSSTRAHLUNG; COHERENT SCATTERING; CRYSTALS; DIFFRACTION; ELECTROMAGNETIC RADIATION; ELEMENTS; MATERIALS HANDLING; MECHANICAL PROPERTIES; METALS; MICROSTRUCTURE; ORIENTATION; RADIATIONS; SCATTERING; TRANSITION ELEMENTS
Optional Information
- Copyright
- Copyright (c) 2011 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.