Published October 1976 | Version v1
Journal article

Preparation and structure of mixed tungsten bronzes containing tin and europium

  • 1. Univ. of Bradford, Eng.

Description

An isothermal section has been established for the system Eu/sub x/WO3-Sn/sub y/WO3 at 10000C from X-ray powder and single-crystal data and Moessbauer spectroscopy and chemical analyses. A single-phase region with the (12 x 3) tetragonal structure has been established. Single-crystal X-ray analysis shows that the Sn and Eu occupy pentagonal tunnel sites. Moessbauer spectroscopy shows that both Sn(II) and Eu(II) are present. The extent of the single-phase field is controlled by two factors: First, the ratio Eu/Sn must be less than 1, and second, the supernumerary electron concentration per WO3 must be less than 0.6

Additional details

Identifiers

Publishing Information

Journal Title
Journal of Solid State Chemistry
Journal Volume
19
Journal Issue
2
Series
J. Solid State Chem.
Journal Page Range
161-167
ISSN
0022-4596

INIS

Country of Publication
United States
Country of Input or Organization
United States
INIS RN
8318112
Subject category
S36: MATERIALS SCIENCE;
Descriptors DEI
CHEMICAL PREPARATION; EUROPIUM COMPOUNDS; MOESSBAUER EFFECT; PHASE STUDIES; POWDERS; TIN COMPOUNDS; TUNGSTATES; VERY HIGH TEMPERATURE; X-RAY SPECTROSCOPY
Descriptors DEC
RARE EARTH COMPOUNDS; SPECTROSCOPY; SYNTHESIS

Optional Information

Notes
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