Electron multiplier for the measurement of an ion current on a mass spectrometer
- 1. Commissariat a l'Energie Atomique, Saclay (France). Centre d'Etudes Nucleaires
Description
The apparatus described is designed to measure weak ion currents received at the collector of a mass spectrometer. The report describes successively the study of electron paths in the multiplier by the method of analogy, using rubber membranes, and the practical details of construction of the apparatus. The variation with surface treatment of the secondary emission coefficient of the alloy CuBe containing 2 per cent Be, which makes up the dynodes, and the influence of the voltage on the gain per stage, are discussed. Results of tests regarding: the influence of the ion mass on the gain, the background of the instrument and the energy distribution of the impulses coming out on a high gain multiplier (q.q. 107) are given. Finally the performances of the multiplier are reported. 1- For a low gain (104), precision and reproducibility comparable to the electrometer valve, sensitivity 100 times greater, currents capable of detection 10-17 Ampere. 2- For a high gain (107) and measurement by impulse counting, currents capable of detection 10-19 Ampere. Mounting difficult to use on a mass spectrometer. (author)
Availability note (English)
Available from INIS in electronic formAbstract (French)
L'appareil decrit est destine a la mesure des faibles courants d'ions re s au collecteur d'un spectrometre de masse. Le rapport decrit successivement l'etude des trajectoires des electrons dans le multiplicateur, par la methode analogique de la menbrane en caoutchouc, et la realisation pratique de l'appareil. La variation du coefficient d'emission secondaire de l'alliage CuBe a 2 pour cent de Be, constituant les dynodes suivant le traitement des surfaces, et l'influence de la tension sur le gain par etage sont discutees. Des resultats d'essais concernant: l'influence de la masse des ions sur le gain, le bruit de fond de l'appareil et la repartition en energie des impulsions de sortie sur un multiplicateur a gain eleve (q.q. 107) sont donnes. Enfin, sont rapportees les performances du multiplicateur. 1- pour un gain faible (104) precision et reproductibilite comparables a la lampe electrometre, sensibilite 100 fois plus grande courants decelables 1O-17 Ampere. 2- pour un gain eleve (107 ) et mesure par comptage d'impulsions, courants decelables 10-19 Ampere. Montage difficilement employable sur un spectrometre de masse. (auteur)Files
38045526.pdf
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Additional details
Additional titles
- Original title (French)
- Multiplicateur d'electrons pour la mesure de courant d'ions sur un spectrometre de masse
Publishing Information
- Imprint Pagination
- 28 p.
- Report number
- CEA-R--692
INIS
- Country of Publication
- France
- Country of Input or Organization
- France
- INIS RN
- 38045526
- Subject category
- S46: INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY;
- Descriptors DEI
- ACCURACY; BACKGROUND NOISE; BERYLLIUM ALLOYS; COPPER BASE ALLOYS; COUNTING TECHNIQUES; DYNODES; ELECTRON MULTIPLIERS; ELECTROPOLISHING; GAIN; ION BEAMS; MASS SPECTROMETERS; MECHANICAL POLISHING; PULSE TECHNIQUES; SECONDARY EMISSION; SENSITIVITY; SURFACE TREATMENTS
- Descriptors DEC
- ALLOYS; AMPLIFICATION; BEAMS; COPPER ALLOYS; ELECTROLYSIS; ELECTRON TUBES; EMISSION; LYSIS; MEASURING INSTRUMENTS; NOISE; POLISHING; SPECTROMETERS; SURFACE FINISHING; TRANSITION ELEMENT ALLOYS
Optional Information
- Notes
- 3 refs.