Modified Bridgman-Stockbarger growth and characterization of LiInSe2 single crystal
Creators
- 1. Centre for Crystal Growth, SSN College of Engineering, Kalavakkam-603110, Tamilnadu (India)
- 2. Materials Science Division, Indira Gandhi Centre for Atomic Research, Kalpakkam-603102, Tamilnadu (India)
Description
The LiInSe2 polycrystalline materials were successfully synthesized from melt and temperature oscillation method. 8 mm diameter and 32 mm length single crystal was grown from Bridgman-Stockbarger method with steady ampoule rotation. Crystalline phase was confirmed by powder XRD pattern. Thermo gravimetric and differential thermal analysis confirms that the melting point of the grown crystal is 897°C. Rutherford backscattering analysis (RBS) gives the crystal composition as Li0.8In1.16Se2.04. The crystalline perfection of the grown crystal was analyzed by High resolution X-ray diffraction measurements (HRXRD). The electrical properties of the grown crystal were analyzed by Hall effect measurements and it confirms the n-type semiconducting nature
Additional details
Identifiers
- DOI
- 10.1063/1.4872910;
Publishing Information
- Journal Title
- AIP Conference Proceedings
- Journal Volume
- 1591
- Journal Issue
- 1
- Journal Page Range
- p. 1223-1225
- ISSN
- 0094-243X
- CODEN
- APCPCS
Conference
- Title
- 58. DAE solid state physics symposium 2013
- Dates
- 17-21 Dec 2013
- Place
- Patiala, Punjab (India)
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 45090507
- Subject category
- S36: MATERIALS SCIENCE; S75: CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- DIFFERENTIAL THERMAL ANALYSIS; ELECTRICAL PROPERTIES; HALL EFFECT; MELTING POINTS; MONOCRYSTALS; POLYCRYSTALS; POWDERS; ROTATION; RUTHERFORD BACKSCATTERING SPECTROSCOPY; STOCKBARGER METHOD; X-RAY DIFFRACTION
- Descriptors DEC
- COHERENT SCATTERING; CRYSTAL GROWTH METHODS; CRYSTALS; DIFFRACTION; MOTION; PHYSICAL PROPERTIES; SCATTERING; SPECTROSCOPY; THERMAL ANALYSIS; THERMODYNAMIC PROPERTIES; TRANSITION TEMPERATURE
Optional Information
- Notes
- (c) 2014 AIP Publishing LLC