Published September 2013 | Version v1
Journal article

Relationship between dislocations and residual stresses in cold-drawn pearlitic steel analyzed by energy-dispersive X-ray diffraction

  • 1. Institute for Materials Research, Tohoku University, Sendai 980-8577 (Japan)
  • 2. Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, Sendai 980-8577 (Japan)
  • 3. Faculty of Engineering, Tokyo City University, Tokyo 158-8557 (Japan)
  • 4. Gyoda 361-0011 (Japan)
  • 5. Japan Synchrotron Radiation Research Institute, Sayo 679-5198 (Japan)
  • 6. Japan Atomic Energy Agency, Sayo 679-5184 (Japan)

Description

We analyzed the dislocation distribution of cold-drawn pearlitic-steel wire by using the line-profile analysis based on the energy dispersive X-ray diffraction (EDXD). Although this line-profile analysis requires a high resolution in reciprocal space, the resolution for EDXD is generally poor due to the energy resolution of the detector. Our analysis demonstrated that the resolution in the reciprocal space can be maximized at small scattering angles. Using the line-profile analysis based on the EDXD, the microstructural parameters such as the crystallite size and the dislocation density of the ferrite phase in the pearlitic steel were successfully analyzed. In addition, the distribution of the residual stress of the ferrite phase of a pearlitic steel wire was also analyzed using the EDXD measurement. - Highlights: • Energy dispersive X-ray diffraction is applied to the line-profile analysis. • Distribution of dislocations in ferrite in the pearlitic steel wire is analyzed. • Relationship between dislocations and residual stress is discussed

Availability note (English)

Available from http://dx.doi.org/10.1016/j.matchar.2013.06.017

Additional details

Identifiers

DOI
10.1016/j.matchar.2013.06.017;
PII
S1044-5803(13)00198-8;

Publishing Information

Journal Title
Materials Characterization
Journal Volume
83
Journal Page Range
p. 152-160
ISSN
1044-5803
CODEN
MACHEX

INIS

Country of Publication
United States
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
45106513
Subject category
S36: MATERIALS SCIENCE;
Descriptors DEI
DISLOCATIONS; ENERGY RESOLUTION; FERRITE; MICROSTRUCTURE; RESIDUAL STRESSES; STEELS; X-RAY DIFFRACTION
Descriptors DEC
ALLOYS; CARBON ADDITIONS; COHERENT SCATTERING; CRYSTAL DEFECTS; CRYSTAL STRUCTURE; DIFFRACTION; IRON ALLOYS; IRON BASE ALLOYS; LINE DEFECTS; RESOLUTION; SCATTERING; STRESSES; TRANSITION ELEMENT ALLOYS

Optional Information

Copyright
Copyright (c) 2013 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.