Formation and quantification of calcium titanate with the perovskite structure from alternative sources of titanium
Creators
- Gralik, G.1
- Raupp-Pereira, F.1
- Hotza, D.1
- Labrincha, J.A.2
- Zanelli, C.3
- Dondi, M.3
- Associacao Brasileira de Ceramica (ABCERAM), Sao Paulo, SP (Brazil)
- Associacao Brasileira de Metalurgia, Materiais e Mineracao (ABM), Sao Paulo, SP (Brazil)
- Associacao Brasileira de Polimeros (ABPol), Sao Carlos, SP (Brazil)
- 1. Universidade Federal de Santa Catarina (UFSC), SC (Brazil)
- 2. Universidade de Aveiro (Portugal)
- 3. Istituto di Scienza e Tecnologia dei Materiali Ceramici (CNR/ISTEC) (Italy)
Description
This study aimed to evaluate and quantify the formation of calcium titanate (CaTiO3) with perovskite structure from alternative sources of titanium (rutile, ilmenite). Commercial raw materials of the high purity were also characterized as reference. With base in the characterization by X-ray fluorescence of the mineral springs different compositions were formulated and subsequently sintered for 2 h in resistive furnace at temperatures in the range 1000 to 1400°C. After thermal processing the samples were analyzed by X-ray diffraction and the quantification of phases formed by the Rietveld method obtained. The results show that the formation and the amount of calcium titanate minerals from alternative sources depend on factors related to stages of sintering and impurities. The microstructures of the compositions were analyzed by SEM/EDS and bulk density also measured. (author)
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48041974.pdf
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Additional details
Publishing Information
- Imprint Pagination
- 8 p.
- Report number
- INIS-BR--17398
Conference
- Title
- Brazilian congress of engineering and materials science
- Original Conference Title
- 21. CBECIMAT: congresso brasileiro de engenharia e ciencia dos materiais
- Acronym
- 21. CBECIMAT
- Dates
- 9-13 Nov 2014
- Place
- Cuiaba, MT (Brazil)
INIS
- Country of Publication
- Brazil
- Country of Input or Organization
- Brazil
- INIS RN
- 48041974
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- BULK DENSITY; CALCIUM; ILMENITE; IMPURITIES; MICROSTRUCTURE; MINERAL SPRINGS; PEROVSKITE; RUTILE; SCANNING ELECTRON MICROSCOPY; SINTERING; TITANATES; X-RAY DIFFRACTION; X-RAY FLUORESCENCE ANALYSIS
- Descriptors DEC
- ALKALINE EARTH METALS; CHEMICAL ANALYSIS; COHERENT SCATTERING; DENSITY; DIFFRACTION; ELECTRON MICROSCOPY; ELEMENTS; FABRICATION; MATERIALS; METALS; MICROSCOPY; MINERALS; NONDESTRUCTIVE ANALYSIS; OXIDE MINERALS; OXYGEN COMPOUNDS; PEROVSKITES; PHYSICAL PROPERTIES; RADIOACTIVE MATERIALS; RADIOACTIVE MINERALS; SCATTERING; TITANIUM COMPOUNDS; TRANSITION ELEMENT COMPOUNDS; WATER SPRINGS; X-RAY EMISSION ANALYSIS