Published 1993 | Version v1
Journal article

Synthesis and NMR study of [4,5,6,8-2H4][2.2]metacyclophane

Description

The synthesis of [4,5,6,8-2H4][2.2]metacyclophane (8) was achieved starting with 2,4,5,6-tetrafluoroisophthalic acid in eight steps in 2% total yield. 1H{2H} and 13C{1H} NMR spectra of 8 showed that the deuterium atoms were introduced at the desired positions. (Author)

Additional details

Publishing Information

Journal Title
Journal of Labelled Compounds and Radiopharmaceuticals
Journal Volume
33
Journal Issue
3
Journal Page Range
p. 205-212.
ISSN
0362-4803
CODEN
JLCRD4

INIS

Country of Publication
United Kingdom
Country of Input or Organization
United Kingdom
INIS RN
24071535
Subject category
S38: RADIATION CHEMISTRY, RADIOCHEMISTRY AND NUCLEAR CHEMISTRY;
Descriptors DEI
AROMATICS; DEUTERIUM COMPOUNDS; LABELLING; NMR SPECTRA
Descriptors DEC
HYDROGEN COMPOUNDS; ORGANIC COMPOUNDS; SPECTRA