Published September 2018
| Version v1
Journal article
Crystal Structure of N-(2-Cyano-1-Phenylprop-2-en-1-yl)-4-Methylbenzenesulfonamide
Creators
- 1. Universidade Federal de Uberlândia (Brazil)
- 2. Universidade Federal de Viçosa (Brazil)
- 3. Universidade Federal de Itajubá (Brazil)
- 4. Universidade de São Paulo (Brazil)
Description
New allylsulfonamide is prepared in a four-step synthetic route: the Morita-Baylis-Hillman adduct prepared from benzaldehyde and acrylonitrile is acetylated using acetic anhydride and DMAP. The acetylated product reacts with DABCO displaced by the addition of 4-methylbenzenesulfonamide. The final product is characterized by high-resolution mass spectrometry, infrared, and NMR spectroscopic techniques. The X-ray crystallographic method is used to determine the crystal structure and features of the molecular structure of the compound.
Additional details
Identifiers
Publishing Information
- Journal Title
- Journal of Structural Chemistry
- Journal Volume
- 59
- Journal Issue
- 5
- Journal Page Range
- p. 1192-1194
- ISSN
- 0022-4766
- CODEN
- JSTCAM
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 55026481
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Descriptors DEI
- ACRYLONITRILE; ANHYDRIDES; BENZALDEHYDE; CRYSTAL STRUCTURE; CRYSTALLOGRAPHY; MASS SPECTROSCOPY; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE; SYNTHESIS; X RADIATION
- Descriptors DEC
- ALDEHYDES; ELECTROMAGNETIC RADIATION; IONIZING RADIATIONS; MAGNETIC RESONANCE; NITRILES; ORGANIC COMPOUNDS; ORGANIC NITROGEN COMPOUNDS; RADIATIONS; RESONANCE; SPECTROSCOPY
Optional Information
- Copyright
- Copyright (c) 2018 Pleiades Publishing, Ltd.