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Published September 2018 | Version v1
Journal article

Crystal Structure of N-(2-Cyano-1-Phenylprop-2-en-1-yl)-4-Methylbenzenesulfonamide

  • 1. Universidade Federal de Uberlândia (Brazil)
  • 2. Universidade Federal de Viçosa (Brazil)
  • 3. Universidade Federal de Itajubá (Brazil)
  • 4. Universidade de São Paulo (Brazil)

Description

New allylsulfonamide is prepared in a four-step synthetic route: the Morita-Baylis-Hillman adduct prepared from benzaldehyde and acrylonitrile is acetylated using acetic anhydride and DMAP. The acetylated product reacts with DABCO displaced by the addition of 4-methylbenzenesulfonamide. The final product is characterized by high-resolution mass spectrometry, infrared, and NMR spectroscopic techniques. The X-ray crystallographic method is used to determine the crystal structure and features of the molecular structure of the compound.

Additional details

Identifiers

Publishing Information

Journal Title
Journal of Structural Chemistry
Journal Volume
59
Journal Issue
5
Journal Page Range
p. 1192-1194
ISSN
0022-4766
CODEN
JSTCAM

Optional Information

Copyright
Copyright (c) 2018 Pleiades Publishing, Ltd.