Published March 2006 | Version v1
Journal article

Obtaining TEM images with a uniform deviation parameter

  • 1. Department of Materials Science and Engineering, Whitaker Laboratory, Lehigh University, 5 East Packer Avenue, Bethlehem, PA 18015-3195 (United States)

Description

In transmission electron microscopes made during the last quarter of a century, it has been impossible to take images in which the diffraction contrast conditions are uniform across the field of view. This is inconvenient when, for example, imaging dislocations at a relatively low magnification. The problem arises because modern microscopes use immersion lenses in which the sample sits in a high magnetic field. The resulting helical trajectories of the electrons at the sample plane mean that it is not possible to make a beam that is parallel at the sample. Results of a method to overcome this problem are presented. It is shown that a simple modification to the microscope (which, on a computer-controlled microscope, could be implemented in software) can be used to produce images in which the deviation parameter is essentially constant across many microns of image. By a happy accident, this method can be used, not only to correct for the helicity imparted by immersion lenses, but also to correct for buckling of the sample (up to a point)

Additional details

Identifiers

DOI
10.1016/j.ultramic.2005.12.002;
PII
S0304-3991(05)00254-8;

Publishing Information

Journal Title
Ultramicroscopy (Amsterdam)
Journal Volume
106
Journal Issue
4-5
Journal Page Range
p. 432-438
ISSN
0304-3991
CODEN
ULTRD6

Optional Information

Copyright
Copyright (c) 2006 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.