Obtaining TEM images with a uniform deviation parameter
Creators
- 1. Department of Materials Science and Engineering, Whitaker Laboratory, Lehigh University, 5 East Packer Avenue, Bethlehem, PA 18015-3195 (United States)
Description
In transmission electron microscopes made during the last quarter of a century, it has been impossible to take images in which the diffraction contrast conditions are uniform across the field of view. This is inconvenient when, for example, imaging dislocations at a relatively low magnification. The problem arises because modern microscopes use immersion lenses in which the sample sits in a high magnetic field. The resulting helical trajectories of the electrons at the sample plane mean that it is not possible to make a beam that is parallel at the sample. Results of a method to overcome this problem are presented. It is shown that a simple modification to the microscope (which, on a computer-controlled microscope, could be implemented in software) can be used to produce images in which the deviation parameter is essentially constant across many microns of image. By a happy accident, this method can be used, not only to correct for the helicity imparted by immersion lenses, but also to correct for buckling of the sample (up to a point)
Additional details
Identifiers
- DOI
- 10.1016/j.ultramic.2005.12.002;
- PII
- S0304-3991(05)00254-8;
Publishing Information
- Journal Title
- Ultramicroscopy (Amsterdam)
- Journal Volume
- 106
- Journal Issue
- 4-5
- Journal Page Range
- p. 432-438
- ISSN
- 0304-3991
- CODEN
- ULTRD6
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 37094315
- Subject category
- S46: INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY;
- Descriptors DEI
- ALIGNMENT; COMPUTER CODES; CONTROL; DESIGN; DIFFRACTION; DISLOCATIONS; ELECTRON MICROSCOPES; ELECTRONS; IMAGES; LENSES; MAGNETIC FIELDS; TRAJECTORIES; TRANSMISSION ELECTRON MICROSCOPY
- Descriptors DEC
- COHERENT SCATTERING; CRYSTAL DEFECTS; CRYSTAL STRUCTURE; ELECTRON MICROSCOPY; ELEMENTARY PARTICLES; FERMIONS; LEPTONS; LINE DEFECTS; MICROSCOPES; MICROSCOPY; SCATTERING
Optional Information
- Copyright
- Copyright (c) 2006 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.