Published January 2013 | Version v1
Journal article

Installation of hybrid ion source on the 1-MV LLNL BioAMS spectrometer

  • 1. Center for Accelerator Mass Spectrometry, Lawrence Livermore National Laboratory, 7000 East Ave, Livermore, CA 94551 (United States)

Description

A second ion source was recently installed onto the LLNL 1-MV AMS spectrometer, which is dedicated to the quantification of 14C and 3H within biochemical samples. This source is unique among the other LLNL cesium sputter ion sources in that it can ionize both gaseous and solid samples. Also, the injection beam line has been designed to directly measure 14C/12C isotope ratios without the need for electrostatic bouncing. Preliminary tests show that this source can ionize transient CO2 gas pulses containing less than 1 μg carbon with approximately 1.5% efficiency. We demonstrate that the measured 14C/12C isotope ratio is largely unaffected by small drifts in the argon stripper gas density. We also determine that a tandem accelerating voltage of 670 kV enables the highest 14C transmission through the system. Finally, we describe a series of performance tests using solid graphite targets spanning nearly 3 orders in magnitude dynamic range and compare the results to our other ion source.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.nimb.2011.11.029

Additional details

Identifiers

DOI
10.1016/j.nimb.2011.11.029;
PII
S0168-583X(11)01060-3;

Publishing Information

Journal Title
Nuclear Instruments and Methods in Physics Research. Section B, Beam Interactions with Materials and Atoms
Journal Volume
294
Journal Page Range
p. 311-314
ISSN
0168-583X
CODEN
NIMBEU

Conference

Title
12. international conference on accelerator mass spectrometry
Dates
20-25 Mar 2011
Place
Wellington (New Zealand)

Optional Information

Copyright
Copyright (c) 2011 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.