Published February 15, 1987 | Version v1
Journal article

Structure of Cs6Zn5(MoO4)8

  • 1. Technische Hochschule Aachen (Germany, F.R.). Lehrstuhl und Inst. fuer Kristallographie

Description

Mr=2403.83, cubic, Ianti 43d (unambiguously determined by X-ray diffraction), a=12.259(1) A, V=1842.32 A3, Z=2, Dm=4.48, Dx=4.3327 g cm-3, λ(CuKα) (for unit-cell dimensions)=1.5418, λ(AgKα) (for intensity measurements)=0.56081 A, μ(AgKα)=138.36 cm-1, F(000)=2144, T=293 K, final R=0.033 for 86 observed reflections. The Mo and Zn atoms form a three-dimensional tetrahedral framework [Mo-O distances 1.694(9)-1.758(9) A, Zn-O distances 1.975(8) A] and the Cs atoms are twelvefold coordinated by O atoms [Cs-O distances 3.273(8)-3.370(8) A], the coordination polyhedron being a distorted cubooctahedron. Refinement of the population factor resulted in 5/6 statistical occupation of the Zn position. (orig.)

Additional details

Publishing Information

Journal Title
Acta Crystallogr., Sect. C: Cryst. Struct. Commun.
Journal Volume
43
Journal Issue
2
Series
Acta Crystallogr., Sect. C: Cryst. Struct. Commun.
Journal Page Range
184-186
ISSN
0108-2701
CODEN
ACSCE