Methodology for determination of benzimidazolic fungicides residues in strawberry and lettuce by HPLC-DAD
Description
systemic fungicides like benzimidazolic compounds are used to protect several crops of fruits and vegetables. in this work a new method for analysis of Benomyl, carbendazim and thiabendazol in strawberry and lettuce by high performance liquid chromatography with diode array detector (HPLC-DAD) was validated. benomyl residues were determined after its conversion to carbendazim. pesticide residues were extracted from strawberry and lettuce samples with ethyl acetate and these extracts were cleaned up by gel permeation chromatography (GPC). final determination was carried out by HPLC-DAD in reverse phase column. the method is selective, specific, precise and accurate. the calibration curves show linearity over concentration range of 1.24 to 6.19 mg/kg, with detection limits of 0.40 and 0.27 mg/kg and quantification limits of 1.35 and 0.81 mg/kg for carbendazim and thiabendazole respectively. the recovery experiments yielding averages of 90 %. n o residues of these compounds were found in collected samples from specific areas of Cundinamarca, Colombia
Additional details
Additional titles
- Original title (Spanish)
- Metodologia para la determinacion de residuos de fungicidas benzimidazolicos en fresa y lechuga por HPLC-DAD
Publishing Information
- Journal Title
- Revista Colombiana de Quimica (Bogota)
- Journal Volume
- 35
- Journal Issue
- 1
- Journal Page Range
- p. 67-79
- ISSN
- 0120-2804
INIS
- Country of Publication
- Colombia
- Country of Input or Organization
- Colombia
- INIS RN
- 39031286
- Subject category
- S62: RADIOLOGY AND NUCLEAR MEDICINE;
- Descriptors DEI
- BENZIMIDAZOLES; COLOMBIA; ECOSYSTEMS; FOOD; FRUITS; FUNGICIDES; HERBICIDES; LETTUCE; ORGANIC COMPOUNDS; PESTICIDES; PLANTS; STRAWBERRIES; VEGETABLES
- Descriptors DEC
- AZOLES; BERRIES; DEVELOPING COUNTRIES; FOOD; FRUITS; HETEROCYCLIC COMPOUNDS; IMIDAZOLES; LATIN AMERICA; MAGNOLIOPHYTA; MAGNOLIOPSIDA; ORGANIC COMPOUNDS; ORGANIC NITROGEN COMPOUNDS; PESTICIDES; PLANTS; ROSACEAE; SOUTH AMERICA; VEGETABLES