Published 2006 | Version v1
Journal article

Methodology for determination of benzimidazolic fungicides residues in strawberry and lettuce by HPLC-DAD

Description

systemic fungicides like benzimidazolic compounds are used to protect several crops of fruits and vegetables. in this work a new method for analysis of Benomyl, carbendazim and thiabendazol in strawberry and lettuce by high performance liquid chromatography with diode array detector (HPLC-DAD) was validated. benomyl residues were determined after its conversion to carbendazim. pesticide residues were extracted from strawberry and lettuce samples with ethyl acetate and these extracts were cleaned up by gel permeation chromatography (GPC). final determination was carried out by HPLC-DAD in reverse phase column. the method is selective, specific, precise and accurate. the calibration curves show linearity over concentration range of 1.24 to 6.19 mg/kg, with detection limits of 0.40 and 0.27 mg/kg and quantification limits of 1.35 and 0.81 mg/kg for carbendazim and thiabendazole respectively. the recovery experiments yielding averages of 90 %. n o residues of these compounds were found in collected samples from specific areas of Cundinamarca, Colombia

Additional details

Additional titles

Original title (Spanish)
Metodologia para la determinacion de residuos de fungicidas benzimidazolicos en fresa y lechuga por HPLC-DAD

Publishing Information

Journal Title
Revista Colombiana de Quimica (Bogota)
Journal Volume
35
Journal Issue
1
Journal Page Range
p. 67-79
ISSN
0120-2804