Published March 1980 | Version v1
Journal article

O17 NMR spectra of diphosphatopolyoxomolybdates

  • 1. AN Kazakhskoj SSR, Alma-Ata. Inst. Khimicheskikh Nauk
  • 2. AN SSSR, Novosibirsk. Inst. Kataliza

Description

Aqueous solutions of the salts Na6P2Mo18O62x52H2O(1), Na4H2P2Mo5O23x10H2O(2) and Na6P2Mo5O23x14H2O(3) with concentration 0.2(1), and 0.4(2)(3) mol/l have been studied using NMR method on the 17O and 31P nuclei. Chemical shifts of 17O and 31P NMR of heteropolyanions P2Mo5O236- and P2Mo18O626- are measured. It is shown that chemical shift of 17O NMR in polyoxomolybdate correlates with the distance to the nearest molybdenum atom

Additional details

Additional titles

Original title (Russian)
Спектры YaMR

Publishing Information

Journal Title
Izv. Akad. Nauk SSSR, Ser. Khim.
Journal Issue
no.3
Series
Izv. Akad. Nauk SSSR, Ser. Khim.
ISSN
0002-3353

INIS

Country of Publication
Russian Federation
Country of Input or Organization
USSR
INIS RN
12629006
Subject category
S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
Descriptors DEI
CHEMICAL SHIFT; HETEROPOLYANIONS; MOLYBDENUM COMPOUNDS; NMR SPECTRA; OXYGEN COMPOUNDS; PHOSPHORUS COMPOUNDS
Descriptors DEC
ANIONS; CHARGED PARTICLES; COMPLEXES; IONS; SPECTRA; TRANSITION ELEMENT COMPOUNDS

Optional Information

Notes
For English translation see the journal Bulletin of the Academy of Sciences USSR, Division of Chemical Science (USA).