Ethylene glycol assisted hydrothermal synthesis of strontium hexaferrite nanoparticles as precursor of magnetic fluid
Creators
- 1. College of Chemistry, Chemical Engineering and Materials Science and Key Laboratory of Organic Synthesis of Jiangsu Province, Soochow University, SIP, Suzhou 215123 (China)
- 2. College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou 350002 (China)
- 3. Suzhou Nanocomp Inc., Suzhou New District, Suzhou 215011 (China)
- 4. Department of Chemical Engineering, University of Waterloo, Waterloo, ON, Canada N2L 3G1 (Canada)
Description
Highlights: ► SrFe12O19 nanoparticles with 25 nm were obtained using EG assisted hydrothermal method. ► SrFe12O19 nanoparticles were modified by oleic acid to form stable magnetic fluid. ► The magnetic fluid had obvious heating effect in an alternating magnetic field. -- Abstract: Strontium hexaferrite (SrFe12O19) nanoparticles were prepared using ethylene glycol (EG) assisted hydrothermal synthesis. The experimental results revealed that the reaction temperature and the amount of EG had an effect on the size, morphology and magnetic properties of SrFe12O19 nanoparticles. SrFe12O19 nanoparticles with a size of about 25 nm were obtained at 140 °C for 24 h at the EG/W volumetric ratios of 1/1. The saturation magnetization of the particles was approximately 10.6 emu/g. Furthermore, SrFe12O19 nanoparticles modified by oleic acid could be dispersed in high boiling point mineral oil to form highly-concentrated magnetic fluid. The magnetic and rheological properties of magnetic fluid were investigated using a Gouy magnetic balance and a rotational rheometer, respectively. The magnetic fluid showed excellent stability in gravity field and external magnetic field, and exhibited shear-thinning behavior. Moreover, the magnetic fluid had obvious heating effect in an alternating magnetic field and had potential on hyperthermia therapy of tumor
Availability note (English)
Available from http://dx.doi.org/10.1016/j.jallcom.2013.02.049Additional details
Identifiers
- DOI
- 10.1016/j.jallcom.2013.02.049;
- PII
- S0925-8388(13)00348-4;
Publishing Information
- Journal Title
- Journal of Alloys and Compounds
- Journal Volume
- 562
- Journal Page Range
- p. 211-218
- ISSN
- 0925-8388
- CODEN
- JALCEU
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 45044016
- Subject category
- S36: MATERIALS SCIENCE; S77: NANOSCIENCE AND NANOTECHNOLOGY;
- Descriptors DEI
- BOILING POINTS; FERRITES; FLUIDS; GLYCOLS; HYDROTHERMAL SYNTHESIS; HYPERTHERMIA; MAGNETIC BALANCES; MAGNETIC FIELDS; MAGNETIC PROPERTIES; MAGNETIZATION; NANOSTRUCTURES; NEOPLASMS; OLEIC ACID; PETROLEUM; SATURATION; STRONTIUM; THERAPY
- Descriptors DEC
- ALCOHOLS; ALKALINE EARTH METALS; BODY TEMPERATURE; CARBOXYLIC ACIDS; DISEASES; ELEMENTS; ENERGY SOURCES; FERRIMAGNETIC MATERIALS; FOSSIL FUELS; FUELS; HYDROXY COMPOUNDS; IRON COMPOUNDS; MAGNETIC MATERIALS; MATERIALS; MEASURING INSTRUMENTS; MEDICINE; METALS; MONOCARBOXYLIC ACIDS; ORGANIC ACIDS; ORGANIC COMPOUNDS; OXYGEN COMPOUNDS; PHYSICAL PROPERTIES; SYNTHESIS; THERMODYNAMIC PROPERTIES; TRANSITION ELEMENT COMPOUNDS; TRANSITION TEMPERATURE
Optional Information
- Copyright
- Copyright (c) 2013 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.