Published February 2012 | Version v1
Journal article

Can the use of pulsed direct current induce oscillation in the applied pressure during spark plasma sintering?

  • 1. Department of Materials and Environmental Chemistry, Arrhenius Laboratory, Stockholm University, S-106 91 Stockholm (Sweden)

Description

The spark plasma sintering (SPS) process is known for its rapid densification of metals and ceramics. The mechanism behind this rapid densification has been discussed during the last few decades and is yet uncertain. During our SPS experiments we noticed oscillations in the applied pressure, related to a change in electric current. In this study, we investigated the effect of pulsed electrical current on the applied mechanical pressure and related changes in temperature. We eliminated the effect of sample shrinkage in the SPS setup and used a transparent quartz die allowing direct observation of the sample. We found that the use of pulsed direct electric current in our apparatus induces pressure oscillations with the amplitude depending on the current density. While sintering Ti samples we observed temperature oscillations resulting from pressure oscillations, which we attribute to magnetic forces generated within the SPS apparatus. The described current–pressure–temperature relations might increase understanding of the SPS process.

Availability note (English)

Available from http://dx.doi.org/10.1088/1468-6996/13/1/015005

Additional details

Publishing Information

Journal Title
Science and Technology of Advanced Materials
Journal Volume
13
Journal Issue
1
Journal Page Range
[6 p.]
ISSN
1468-6996

INIS

Country of Publication
United Kingdom
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
43120247
Subject category
S36: MATERIALS SCIENCE;
Descriptors DEI
CERAMICS; CURRENT DENSITY; DIRECT CURRENT; METALS; OSCILLATIONS; PLASMA; QUARTZ; SINTERING
Descriptors DEC
CURRENTS; ELECTRIC CURRENTS; ELEMENTS; FABRICATION; MINERALS; OXIDE MINERALS