Published January 2013 | Version v1
Journal article

Extraction of topographic and material contrasts on surfaces from SEM images obtained by energy filtering detection with low-energy primary electrons

  • 1. Steel Research Laboratory, JFE Steel Corporation, 1 Kawasaki-cho, Chuo-ku, Chiba 260-0835 (Japan)
  • 2. Steel Research Laboratory, JFE Steel Corporation, 1 Kohkan-cho, Fukuyama 721-8510 (Japan)

Description

Secondary electron microscope (SEM) images have been obtained for practical materials using low primary electron energies and an in-lens type annular detector with changing negative bias voltage supplied to a grid placed in front of the detector. The kinetic-energy distribution of the detected electrons was evaluated by the gradient of the bias-energy dependence of the brightness of the images. This is divided into mainly two parts at about 500 V, high and low brightness in the low- and high-energy regions, respectively and shows difference among the surface regions having different composition and topography. The combination of the negative grid bias and the pixel-by-pixel image subtraction provides the band-pass filtered images and extracts the material and topographic information of the specimen surfaces. -- Highlights: ► Scanning electron (SE) images contain many kind of information on material surfaces. ► We investigate energy-filtered SE images for practical materials. ► The brightness of the images is divided into two parts by the bias voltage. ► Topographic and material contrasts are extracted by subtracting the filtered images.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.ultramic.2012.08.011

Additional details

Identifiers

DOI
10.1016/j.ultramic.2012.08.011;
PII
S0304-3991(12)00215-X;

Publishing Information

Journal Title
Ultramicroscopy (Amsterdam)
Journal Volume
124
Journal Page Range
p. 20-25
ISSN
0304-3991
CODEN
ULTRD6

INIS

Country of Publication
Netherlands
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
45028044
Subject category
S36: MATERIALS SCIENCE;
Descriptors DEI
ELECTRIC POTENTIAL; ELECTRON SPECTRA; ELECTRONS; ENERGY DEPENDENCE; FILTERS; IMAGE PROCESSING; IMAGES; SCANNING ELECTRON MICROSCOPY; SURFACES; TOPOGRAPHY
Descriptors DEC
ELECTRON MICROSCOPY; ELEMENTARY PARTICLES; FERMIONS; LEPTONS; MICROSCOPY; PROCESSING; SPECTRA

Optional Information

Copyright
Copyright (c) 2012 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.