Published April 1, 1986 | Version v1
Journal article

Post-refinement of oscillation diffraction data collected at a synchrotron radiation source

  • 1. Purdue Univ., Lafayette, IN (USA). Dept. of Biological Sciences
  • 2. Cornell Univ., Ithaca, NY (USA). Section of Biochemistry, Molecular and Cell Biology

Description

''Post-refinement'' is a technique used to compare the intensity of partially recorded reflections on oscillation photographs with their full intensity observed elsewhere on the same or a different film. A reflection's partiality depends on crystal orientation, crystal cell dimension and crystal mosaicity, and post-refinement is a very sensitive tool for the refinement of these parameters. A previous paper describes how post-refinement can be applied to data derived from a set of oscillation films. In this paper the technique has been extended to the refinement of anisotropic beam divergence and wavelength dispersion as is normally found on synchrotron sources. In an example it is shown that post-refinement is sufficiently sensitive to detect small wavelength variations due to changes in temperature of the monochromating crystal. (orig.)

Additional details

Publishing Information

Journal Title
J. Appl. Crystallogr.
Journal Volume
19
Journal Issue
2
Series
J. Appl. Crystallogr.
Journal Page Range
134-139
ISSN
0021-8898
CODEN
JACGA