Post-refinement of oscillation diffraction data collected at a synchrotron radiation source
- 1. Purdue Univ., Lafayette, IN (USA). Dept. of Biological Sciences
- 2. Cornell Univ., Ithaca, NY (USA). Section of Biochemistry, Molecular and Cell Biology
Description
''Post-refinement'' is a technique used to compare the intensity of partially recorded reflections on oscillation photographs with their full intensity observed elsewhere on the same or a different film. A reflection's partiality depends on crystal orientation, crystal cell dimension and crystal mosaicity, and post-refinement is a very sensitive tool for the refinement of these parameters. A previous paper describes how post-refinement can be applied to data derived from a set of oscillation films. In this paper the technique has been extended to the refinement of anisotropic beam divergence and wavelength dispersion as is normally found on synchrotron sources. In an example it is shown that post-refinement is sufficiently sensitive to detect small wavelength variations due to changes in temperature of the monochromating crystal. (orig.)
Additional details
Publishing Information
- Journal Title
- J. Appl. Crystallogr.
- Journal Volume
- 19
- Journal Issue
- 2
- Series
- J. Appl. Crystallogr.
- Journal Page Range
- 134-139
- ISSN
- 0021-8898
- CODEN
- JACGA
INIS
- Country of Publication
- Denmark
- Country of Input or Organization
- Denmark
- INIS RN
- 17056223
- Subject category
- S75: CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY;
- Descriptors DEI
- ANISOTROPY; CRYSTALS; DATA ACQUISITION; DISPERSION RELATIONS; FILMS; MOSAICISM; ORIENTATION; OSCILLATIONS; RADIATION SOURCES; REFINING; SYNCHROTRON RADIATION; X-RAY DIFFRACTION
- Descriptors DEC
- BREMSSTRAHLUNG; COHERENT SCATTERING; DIFFRACTION; ELECTROMAGNETIC RADIATION; RADIATIONS; SCATTERING