Published January 2021 | Version v1
Journal article

Orientation and deformation conditions dependence of dislocation substructures in cold deformed pure tantalum

  • 1. MINES ParisTech, PSL Research University, CEMEF - Centre de mise en forme des matériaux, CNRS UMR 7635, CS 10207 rue Claude Daunesse, 06904 Sophia Antipolis Cedex (France)
  • 2. CEA DAM Valduc, F-21120 Is-sur-Tille (France)

Description

Highlights: • Deformed microstructures of pure tantalum were studied and modelled. • The γ-fiber texture is stable during compression but not during rolling. • Dislocation substructures form intensely in γ-fiber, and not at all in θ-fiber. • Substructures formation depends on the intensity of γ-fiber in the initial state. • Close dislocation densities in γ-fiber can lead to different substructures states. The evolution of dislocation arrangement during deformation can lead to the development of dislocation substructures which have direct consequences on the subsequent microstructural evolutions. Dislocation densities and substructures of various deformed microstructures of pure tantalum are analyzed in order to study the influence of deformation conditions. Electron BackScatter Diffraction (EBSD) and Electron Channeling Contrast Imaging (ECCI) are used in order to characterize the development of dislocation substructures. Investigation at grain scale shows the orientation dependence of the deformed state with the highest dislocation content for γ-fiber grains. This fiber appears to be quite stable in compression but less in rolling. Investigation at dislocation substructure scale highlights the influence of orientation on dislocation substructure forming. Developed substructures are present in the interior of γ-fiber grains. The evolution of the disorientation and size of substructures with strain depends greatly on the initial fraction of γ-fiber in the microstructure. Models describing these evolutions are proposed for γ-fiber grains. On the basis of the present analysis it is concluded that dislocation density parameter does not allow transcribing the differences of substructural development.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.matchar.2020.110789

Additional details

Identifiers

DOI
10.1016/j.matchar.2020.110789;
PII
S1044580320322609;

Publishing Information

Journal Title
Materials Characterization
Journal Volume
171
Journal Page Range
vp.
ISSN
1044-5803
CODEN
MACHEX

Optional Information

Copyright
Copyright (c) 2020 Elsevier Inc. All rights reserved.