Published February 1985 | Version v1
Journal article

Preparation, structure, and thermal behaviour of a new Ge-W bronce

Creators

  • 1. Giessen Univ. (Germany, F.R.)

Description

A hexagonal Ge-tungsten bronce with the composition Ge/sub 0.24/WO3 is obtained by chemical vapour deposition of a mixture of GeO2 and WO2 (temperature gradient: 930 to 830 0C). By means of a X-ray crystal structure analysis the space group was determined to be P622 and the lattice constants a = 744.0 pm, c = 381.7 pm. In absence of oxygen Ge/sub 0.24/WO3 is stable up to 850 0C; in contact with air it is oxydized at temperatures T > 670 0C. An anomaly in the thermal lattice expansion at temperatures T > 260 0C is discussed. (author)

Additional details

Additional titles

Original title (German)
Darstellung, Struktur und thermisches Verhalten einer neuen hexagonalen Ge-W-Bronze

Publishing Information

Journal Title
Z. Anorg. Allg. Chem.
Journal Volume
521
Series
Z. Anorg. Allg. Chem.
Journal Page Range
191-198
ISSN
0044-2313