Published May 1976
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Determination of dibutylbutylphosphonate in the presence of tributylphosphate by gas liquid chromatography
Description
A gas chromatographic determination of dibutylbutyl-phosphonate in the presence of tributylphosphate was developed. The separation was done on a 183 cm by 3 mm stainless steel column packed with 10 percent Carbowax 20M--TPA on 80/100 mesh Chromosorb W AW and detected by flame ionization. A nitrogen carrier gas flow of 40 cm3/min and an oven temperature of 1800C produced optimum resolution and column efficiency. The use of temperature programming reduced retention times and thus analysis time. An internal standard of 10 percent v/v n-tridecane was added to all samples and standards
Availability note (English)
MF available from INIS under the Report Number.Files
8289130.pdf
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Additional details
Publishing Information
- Imprint Pagination
- 25 p.
- Report number
- ARH-SA--249
Conference
- Title
- 31. annual northwest regional American Chemical Society meeting.
- Dates
- 14 Jun 1976.
- Place
- Reno, Nevada, United States of America (USA).
INIS
- Country of Publication
- United States
- Country of Input or Organization
- United States
- INIS RN
- 8289130
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; S11: NUCLEAR FUEL CYCLE AND FUEL MATERIALS;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- GAS CHROMATOGRAPHY; PHOSPHORIC ACID ESTERS; QUANTITY RATIO; TBP; TEMPERATURE DEPENDENCE
- Descriptors DEC
- BUTYL PHOSPHATES; CHROMATOGRAPHY; ESTERS; ORGANIC COMPOUNDS; ORGANIC PHOSPHORUS COMPOUNDS; SEPARATION PROCESSES
Optional Information
- Notes
- Available from NTIS. $4.00.
- Secondary number(s)
- CONF-760668--1.