Published September 1977 | Version v1
Journal article

Synthesis and characterization of the difluorotris (fluorosulfate of uranium (V): UF2(SO3F)3

  • 1. Centre d'Etudes Nucleaires de Saclay, Gif-sur-Yvette, France

Description

A new U(V) compound, UF2(SO3F)3, has been synthesized by the reaction of UF6 and SO3 in both the gaseous phase and CFCl3 solution. This leads to a blue-green solid, the x-ray powder diffraction pattern of which has been recorded. Its oxidation state has been deduced from chemical analysis, the electronic absorption spectrum, and magnetic measurements. The environment around uranium is discussed from Raman and infrared spectra recorded at ambient and liquid nitrogen temperatures

Additional details

Identifiers

Publishing Information

Journal Title
Inorganic Chemistry
Journal Volume
16
Journal Issue
9
Series
Inorg. Chem.
Journal Page Range
2252-2257
ISSN
0020-1669

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