High-rate formation of nano-scale alumina particles
- 1. Div. of Engineering, Brown Univ., Providence, RI (United States)
Description
In this paper the authors report a new approach to the problem of high rate formation of nanophase powders. In experiments the authors were able to make aluminium oxide particles in the size range from 5 to 140 nm (peaking sharply at 34 nm) at a rate of 3 g/min. The starting material was a mixture of aluminum-tri-sec-butoxide and sec-butanol. An aerosol was made from this solution and subsequently burned in a special torch, described below. The resulting particles were spherical and no necked regions were observable between them. In a practical application, our technique allows a large production rate while still approaching the ideal of nano-scale mono-scale monodispersed particles. The work was extended to the formation of zirconium oxide particles with quite similar results in the size distribution
Additional details
Publishing Information
- Publisher
- Materials Research Society.
- Imprint Place
- New York, NY (United States)
- ISBN
- 1-55899-143-3
- Imprint Title
- Proceedings of the synthesis and processing of ceramics emdash scientific issues
- Imprint Pagination
- 585 p.
- Journal Page Range
- p. 145-152.
Conference
- Title
- Annual fall meeting of the Materials Research Society.
- Dates
- 2-6 Dec 1991.
- Place
- Boston, MA (United States).
INIS
- Country of Publication
- United States
- Country of Input or Organization
- United States
- INIS RN
- 24010009
- Subject category
- S36: MATERIALS SCIENCE;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- ALUMINIUM OXIDES; CHEMICAL PREPARATION; CHEMICAL REACTION KINETICS; COMBUSTION; FABRICATION; PARTICLE SIZE; POWDERS; SOLID SOLUTIONS; ZIRCONIUM OXIDES
- Descriptors DEC
- ALUMINIUM COMPOUNDS; CHALCOGENIDES; CHEMICAL REACTIONS; DISPERSIONS; HOMOGENEOUS MIXTURES; KINETICS; MIXTURES; OXIDATION; OXIDES; OXYGEN COMPOUNDS; REACTION KINETICS; SIZE; SOLUTIONS; SYNTHESIS; TRANSITION ELEMENT COMPOUNDS; ZIRCONIUM COMPOUNDS
Optional Information
- Secondary number(s)
- CONF-911202--.