Published 2006
| Version v1
Journal article
Using solid-state 13C NMR to follow up the synthesis of a new bioactive N-acyl hydrazone
- 1. Universidade Federal do Rio de Janeiro (UFRJ), RJ (Brazil). Inst. de Quimica. Dept. de Quimica Organica
- 2. Universidade Federal do Rio de Janeiro (UFRJ), RJ (Brazil). Faculdade de Farmacia. LASSBio
Description
In this communication, solid state 13C NMR is used as a follow up technique for the synthesis of a new N-acyl hydrazone with very low solubility in most common solvents. Both cross-polarization magic angle spinning without and with interrupted decoupling were employed. It was possible to confirm that the coupling reaction furnished the desired new hydrazone.(author)
Availability note (English)
Available from http://www.auremn.org.br/Annals/2006-vol5-num1/AMR0082006_34-40.pdfAdditional details
Identifiers
Publishing Information
- Journal Title
- Annals of Magnetic Resonance
- Journal Volume
- 5
- Journal Issue
- 1/3
- Journal Page Range
- p. 34-40
- ISSN
- 1519-8308
INIS
- Country of Publication
- Brazil
- Country of Input or Organization
- Brazil
- INIS RN
- 39070324
- Subject category
- S75: CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY;
- Descriptors DEI
- ALDEHYDES; CARBON; CARBON 13; HYDRAZINE; HYDRAZONES; NMR SPECTRA; NUCLEAR MAGNETIC RESONANCE; ORGANIC SOLVENTS; SOLVENTS; STRUCTURAL CHEMICAL ANALYSIS
- Descriptors DEC
- CARBON ISOTOPES; ELEMENTS; EVEN-ODD NUCLEI; ISOTOPES; LIGHT NUCLEI; MAGNETIC RESONANCE; NITROGEN COMPOUNDS; NONAQUEOUS SOLVENTS; NONMETALS; NUCLEI; ORGANIC COMPOUNDS; ORGANIC NITROGEN COMPOUNDS; RESONANCE; SOLVENTS; SPECTRA; STABLE ISOTOPES
Optional Information
- Notes
- 7 refs., 5 figs., 1 tab.