Published October 2011
| Version v1
Report
Sonochemical synthesis of SnO2 nanocrystals
Creators
- 1. Instituto Peruano de Energia Nuclear, Lima (Peru). Direccion de Investigacion y Desarrollo
- 2. Universidad Nacional de Ingenieria, Lima (Peru). Facultad de Ciencias
Description
This paper presents the preliminary results of obtaining of SnO2 nanocrystals. Irradiating an aqueous solution of 0.13M SnCl4.5(H2O) with ultrasounds during 150 min at a temperature of 65 oC, and using as a precipitant ammonia 25 % was obtained SnO2 nanocrystals with a crystallite size of 2 nm. The SnO2 nanocrystals efficiency is 92 %, these nanocrystals were characterized by X-ray diffraction, scanning and transmission electron microscopy. The crystallite size of SnO2 nanocrystals was determined using the TOPAS ACADEMIC software. (orig.)
Additional details
Additional titles
- Original title (Spanish)
- Sintesis Sonoquimica de nanocristales de SnO
Publishing Information
- Imprint Title
- Scientific and Technological Report 2010
- Imprint Pagination
- 236 p.
- Journal Page Range
- p. 55-58
- ISSN
- 1684-1662
- Report number
- INIS-PE--049
INIS
- Country of Publication
- Peru
- Country of Input or Organization
- Peru
- INIS RN
- 43119167
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- AQUEOUS SOLUTIONS; CRYSTALS; NANOSTRUCTURES; SYNTHESIS; TIN OXIDES; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION
- Descriptors DEC
- CHALCOGENIDES; COHERENT SCATTERING; DIFFRACTION; DISPERSIONS; ELECTRON MICROSCOPY; HOMOGENEOUS MIXTURES; MICROSCOPY; MIXTURES; OXIDES; OXYGEN COMPOUNDS; SCATTERING; SOLUTIONS; TIN COMPOUNDS
Optional Information
- Notes
- 10 refs., 2 figs., 1 tab. Imprint:Informe Cientifico Tecnologico 2010